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3,5-双（4-氟苯基）-1-（4-硝基苯基）-4,5-二氢-1H-吡唑

3,5-Bis(4-fluoro-phen-yl)-1-(4-nitro-phen-yl)-4,5-dihydro-1H-pyrazole.

作者信息

Samshuddin Seranthimata, Narayana Badiadka, Yathirajan Hemmige S, Gerber Thomas, Hosten Eric, Betz Richard

机构信息

Mangalore University, Department of Studies in Chemistry, Mangalagangotri 574 199, India.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2012 Nov 1;68(Pt 11):o3216-7. doi: 10.1107/S160053681204370X. Epub 2012 Oct 27.

DOI:10.1107/S160053681204370X
PMID:23284522
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3515302/
Abstract

In the title compound, C(21)H(15)F(2)N(3)O(2), a pyrazole derivative bearing three aromatic substituents, the central five-membered heterocyclic ring makes dihedral angles of 1.77 (14), 3.68 (13) and 72.15 (14)° with the three benzene rings. In the crystal, C-H⋯O and C-H⋯F inter-actions connect the mol-ecules into double layers parallel to the bc plane.

摘要

在标题化合物C₂₁H₁₅F₂N₃O₂中，这是一种带有三个芳基取代基的吡唑衍生物，中心五元杂环与三个苯环形成的二面角分别为1.77 (14)°、3.68 (13)°和72.15 (14)°。在晶体中，C—H⋯O和C—H⋯F相互作用将分子连接成平行于bc平面的双层结构。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3221/3515302/98143c9d67d1/e-68-o3216-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3221/3515302/903a4f3bfbd1/e-68-o3216-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3221/3515302/d968c7be3cf1/e-68-o3216-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3221/3515302/98143c9d67d1/e-68-o3216-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3221/3515302/903a4f3bfbd1/e-68-o3216-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3221/3515302/d968c7be3cf1/e-68-o3216-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3221/3515302/98143c9d67d1/e-68-o3216-fig3.jpg

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