Karaarslan Emine Sirin, Bulbul Mehmet, Ertas Ertan, Cebe Mehmet Ata, Usumez Aslihan
Department of Restorative Dentistry, Faculty of Dentistry, Gaziantep University, Gaziantep, TURKIYE.
Eur J Dent. 2013 Jan;7(1):110-6.
To examine the amount of change in color and color parameters of a composite resin (Filtek P60) polymerized by five different polymerization methods.
A Teflon mold (6mm in diameter, 2mm in height) was used to prepare the composite resin discs (n=10). G1: Polymerization with inlay oven; G2: Polymerization with HQTH and autoclave; G3: Polymerization with LED and autoclave; G4: Polymerization with HQTH; G5: Polymerization with LED. Colorimetric values of the specimens before and after polymerization were measured using a spectrophotometer. The CIE Lab color system was used for the determination of color difference. Analysis of variance (ANOVA) was used to analyze the data for significant differences. Tukey's HSD test and paired two-tailed tests were used to perform multiple comparisons (α=.05).
There were no significant differences in total color change (ΔEab) among the polymerization groups (P>.05). However, the lowest color change (ΔEab) value was 3.3 in LED and autoclave; the highest color change (ΔEab) value was 4.6 in HQTH. For all groups, CIE L, Cab and avalues decreased after polymerization (P<.05). The highest Δb* and ΔC*ab values were observed in specimens polymerized in an inlay oven (P<.05).
Composite resin material showed color changes above the clinically accepted value in all study groups (ΔEab⩾3.3). All specimens became darker during investigation (ΔL< 0). Specimens polymerized with inlay oven presented the highest Δb* values which means less yellow color in specimens.
研究采用五种不同聚合方法聚合的复合树脂(Filtek P60)的颜色及颜色参数变化量。
使用聚四氟乙烯模具(直径6mm,高2mm)制备复合树脂圆盘(n = 10)。G1:用嵌体炉聚合;G2:用高强度卤钨灯(HQTH)和高压釜聚合;G3:用发光二极管(LED)和高压釜聚合;G4:用HQTH聚合;G5:用LED聚合。聚合前后样本的比色值用分光光度计测量。采用CIE Lab颜色系统测定色差。用方差分析(ANOVA)分析数据有无显著差异。采用Tukey's HSD检验和配对双尾检验进行多重比较(α = 0.05)。
各聚合组之间的总颜色变化(ΔEab)无显著差异(P > 0.05)。然而,LED和高压釜聚合组的颜色变化(ΔEab)值最低,为3.3;HQTH聚合组的颜色变化(ΔEab)值最高,为4.6。所有组在聚合后CIE L、Cab和a值均降低(P < 0.05)。在嵌体炉中聚合的样本中观察到最高的Δb和ΔCab值(P < 0.05)。
在所有研究组中,复合树脂材料的颜色变化均高于临床可接受值(ΔEab⩾3.3)。在研究过程中所有样本均变深(ΔL < 0)。用嵌体炉聚合的样本呈现最高的Δb*值,这意味着样本中的黄色较少。