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黏结剂老化对自黏结剂黏固桩黏结界面的影响:为期 1 年的研究。

Aging affects the adhesive interface of posts luted with self-adhesive cements: a 1-year study.

机构信息

Department of Medical Sciences, University of Trieste, Trieste, Italy.

出版信息

J Adhes Dent. 2013 Apr;15(2):173-80. doi: 10.3290/j.jad.a28387.

Abstract

PURPOSE

To examine the bond strength and interfacial nanoleakage expression of fiber posts luted to intraradicular dentin with self-adhesive cements. Six-month and 1-year aging effects were examined.

MATERIALS AND METHODS

Post space was created in endodontically treated human incisors. Each tooth was assigned to a self-adhesive cement/post combination: (1) Bifix SE Cement (Voco) with proprietary posts (Rebilda Post, Voco), (2) RelyX Unicem (3M ESPE) with proprietary posts (Rely X Fiber Post, 3M ESPE), (3) MaxCem (Kerr) with Rebilda Posts. Each specimen was cut into 1-mm-thick sections and either immediately stressed to failure with the push-out bond strength test or aged in artificial saliva for 6 months or 1 year before testing. Additional specimens were processed for quantitative interfacial nanoleakage analysis using ammoniacal silver nitrate.

RESULTS

Immediate bond strength ranked in the following order: Bifix SE (7.8 ± 2.9 MPa) = RelyX Unicem (8.4 ± 2.7 MPa) > MaxCem (4.6 ± 2.4 MPa) (p < 0.05). Aging significantly reduced the bond strength of all cements after 1 year: Bifix SE (3.8 ± 1.4 MPa) = RelyX Unicem (5.8 ± 1.7 MPa) > MaxCem (1.3 ± 0.9 MPa; p<0.05). No immediate difference in interfacial nanoleakage expression was found. Nanoleakage increased after aging, and MaxCem showed the highest values.

CONCLUSION

The push-out strength and interfacial nanoleakage expression of fiber posts luted with self-adhesive cements were dependent on luting material and type of post, and were significantly affected by storage time.

摘要

目的

研究自粘接水泥粘结到根管内牙本质的纤维桩的粘结强度和界面纳米渗漏表达,并检查 6 个月和 1 年老化的影响。

材料和方法

在牙髓治疗过的人切牙中创建桩腔。将每颗牙齿分配到一种自粘接水泥/桩组合:(1)Bifix SE 水泥(Voco)与专用桩(Rebilda 桩,Voco),(2)RelyX Unicem(3M ESPE)与专用桩(RelyX 纤维桩,3M ESPE),(3)MaxCem( Kerr)与 Rebilda 桩。每个标本均切成 1 毫米厚的切片,立即用推出粘结强度测试进行失效应力测试,或在人工唾液中老化 6 个月或 1 年后进行测试。使用氨硝酸银对其他标本进行定量界面纳米渗漏分析。

结果

即刻粘结强度的顺序如下:Bifix SE(7.8 ± 2.9 MPa)= RelyX Unicem(8.4 ± 2.7 MPa)> MaxCem(4.6 ± 2.4 MPa)(p < 0.05)。1 年后,所有水泥的粘结强度均明显降低:Bifix SE(3.8 ± 1.4 MPa)= RelyX Unicem(5.8 ± 1.7 MPa)> MaxCem(1.3 ± 0.9 MPa;p < 0.05)。即时界面纳米渗漏表达无差异。老化后纳米渗漏增加,MaxCem 显示最高值。

结论

自粘接水泥粘结纤维桩的推出强度和界面纳米渗漏表达取决于粘结材料和桩的类型,并受储存时间的显著影响。

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