Cadd S J, Bleay S M, Sears V G
School of Science and Engineering, Teesside University, Middlesbrough, UK.
Sci Justice. 2013 Jun;53(2):131-43. doi: 10.1016/j.scijus.2012.11.007. Epub 2012 Dec 28.
A comparison is reported of the relative effectiveness to two formulations of the solvent black 3 (Sudan Black) reagent used to enhance grease contaminated fingermarks. These experiments compared the currently recommended ethanol-based formulation with a lower flammability system based on 1-methoxy-2-propanol (PGME) using natural, deliberately sebaceous and grease contaminated marks across a range of surfaces. It is shown that overall the PGME-based formulation was significantly better at producing good ridge detail on most surfaces for both natural and deliberately sebaceous prints, and for contaminated prints the ridge detail obtained with the PGME-based formulation was as good or better than that obtained with the ethanol formulation. Several smaller experiments were also carried out in order to provide additional information on the solvent black 3 process. These showed that solutions of age up to 2 years can still develop good ridge detail, but the colour of the stained mark may vary. It was also demonstrated that the currently recommended 2 minute treatment time often resulted in very heavy background staining and in practice significantly reduced treatment times can be recommended according to the nature of the surface present.
本文报道了用于增强油脂污染指纹的溶剂黑3(苏丹黑)试剂两种配方的相对有效性比较。这些实验将目前推荐的乙醇基配方与基于1-甲氧基-2-丙醇(PGME)的低易燃性体系进行了比较,使用了在一系列表面上的自然、故意皮脂腺分泌和油脂污染的指纹。结果表明,总体而言,基于PGME的配方在大多数表面上,对于自然和故意皮脂腺分泌的指纹,在产生良好的纹路细节方面明显更好,对于污染指纹,基于PGME的配方获得的纹路细节与乙醇配方相当或更好。还进行了几个较小的实验,以提供关于溶剂黑3工艺的更多信息。这些实验表明,长达2年的溶液仍能产生良好的纹路细节,但染色指纹的颜色可能会有所不同。还证明了目前推荐的2分钟处理时间常常导致背景染色过重,实际上根据存在的表面性质,可以推荐显著缩短的处理时间。