Lee Seong-Hee, Jeon Jae-Yeol, Lee Kwang-Jin
Department of Advanced Materials Science and Engineering, Mokpo National University, Muan-gun 534-729, Chonnam, Korea.
J Nanosci Nanotechnol. 2013 Jan;13(1):509-12. doi: 10.1166/jnn.2013.6924.
An ultrafine grain (UFG) complex lamella aluminum alloy sheet was successfully fabricated by ARB process using AA1050 and AA6061. The lamella thickness of the alloy became thinner and elongated to the rolling direction with increasing the number of ARB cycles. By TEM observation, it is revealed that the aspect ratio of UFGs formed by ARB became smaller with increasing the number of ARB cycles. In addition, the effect of ARB process on the development of deformation texture at the quarter thickness of ARB-processed sheets was clarified. ARB process leaded to the formation of the rolling texture with shear texture and weak cube orientation. The subdivision of the grains to the rolling direction began to occur after 3 cycles of the ARB, resulting in formation of ultrafine grains with small aspect ratio. After 5 cycles, the ultrafine grained structure with the average grain diameter of 560 nm develops in almost whole regions of the sample.
采用AA1050和AA6061通过累积叠轧(ARB)工艺成功制备了一种超细晶粒(UFG)复合层状铝合金板材。随着ARB循环次数的增加,合金的层片厚度变薄并沿轧制方向拉长。通过透射电子显微镜(TEM)观察发现,随着ARB循环次数的增加,由ARB形成的UFG的纵横比变小。此外,还阐明了ARB工艺对ARB处理板材四分之一厚度处变形织构发展的影响。ARB工艺导致形成具有剪切织构和弱立方取向的轧制织构。在ARB进行3次循环后,晶粒开始沿轧制方向细分,从而形成纵横比小的超细晶粒。5次循环后,平均晶粒直径为560 nm的超细晶粒结构在样品的几乎整个区域中形成。