Suppr超能文献

(1S,3R,8R,9S,11R)-2,2-Di-bromo-10,10-di-chloro-3,7,7,11-tetra-methyl-tetra-cyclo-[6.5.0.0(1,3).0(9,11)]trideca-ne.

作者信息

Ourhriss Najia, Benharref Ahmed, Saadi Mohamed, Berraho Moha, El Ammari Lahcen

机构信息

Laboratoire de Chimie Biomoléculaire, Substances Naturelles et Réactivité "Unité Associée au CNRST (URAC16)", Université Cadi Ayyad, Faculté des Sciences Semlalia, BP 2390, Bd My Abdellah, 40000 Marrakech, Morocco.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2013 Apr 13;69(Pt 5):o724. doi: 10.1107/S1600536813009070. Print 2013 May 1.

Abstract

The title compound, C17H24Br2Cl2, was synthesized from β-himachalene (3,5,5,9-tetra-methyl-2,4a,5,6,7,8-hexa-hydro-1H-benzo-cyclo-heptene), which was isolated from the essential oil of the Atlas cedar (Cedrus Atlantica). The mol-ecule contains fused six-, seven- and two three-membered rings. The six-membered ring has a half-chair conformation, while the seven-membered ring displays a boat conformation. The absolute structure was unambiguously established from anomalous dispersion effects. The crystal packing exhibits no short inter-molecular contacts.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f9e3/3648256/dc2ad9655720/e-69-0o724-fig1.jpg

相似文献

1
(1S,3R,8R,9S,11R)-2,2-Di-bromo-10,10-di-chloro-3,7,7,11-tetra-methyl-tetra-cyclo-[6.5.0.0(1,3).0(9,11)]trideca-ne.
Acta Crystallogr Sect E Struct Rep Online. 2013 Apr 13;69(Pt 5):o724. doi: 10.1107/S1600536813009070. Print 2013 May 1.
2
(1S,3R,8R,9S,11R)-10,10-Di-bromo-2,2-di-chloro-3,7,7,11-tetra-methyl-tetra-cyclo-[6.5.0.0(1,3).0(9,11)]trideca-ne.
Acta Crystallogr Sect E Struct Rep Online. 2013 Apr 17;69(Pt 5):o739. doi: 10.1107/S1600536813010040. Print 2013 May 1.
3
(1S,3S,8R,9S,11R)-10,10-Di-chloro-3,7,7,11-tetra-methyl-tetra-cyclo[6.5.0.0(1,3).0(9,11)]trideca-ne.
Acta Crystallogr Sect E Struct Rep Online. 2013 May 22;69(Pt 6):o933-4. doi: 10.1107/S1600536813013457. Print 2013 Jun 1.
4
(1S,3S,8R,9S,11R)-10,10-Di-bromo-3,7,7,11-tetra-methyl-tetra-cyclo-[6.5.0.0(1,3).0(9,11)]trideca-ne.
Acta Crystallogr Sect E Struct Rep Online. 2013 Jul 13;69(Pt 8):o1261. doi: 10.1107/S160053681301903X. eCollection 2013.
5
(1S,3R,8R,9S,11R)-2,2,10,10-Tetra-chloro-3,7,7,11-tetra-methyl-tetra-cyclo-[6.5.0.0(1,3).0(9,11)]trideca-ne.
Acta Crystallogr Sect E Struct Rep Online. 2013 Feb 1;69(Pt 2):o275. doi: 10.1107/S1600536813001700. Epub 2013 Jan 23.
6
Crystal structure of (1S,3R,8R,9S,10R)-10-bromo-methyl-2,2-di-chloro-9,10-ep-oxy-3,7,7-tri-methyl-tri-cyclo-[6.4.0.0(1,3)]dodeca-ne.
Acta Crystallogr E Crystallogr Commun. 2015 Apr 9;71(Pt 5):o284-5. doi: 10.1107/S205698901500657X. eCollection 2015 May 1.
7
2,2-Dichloro-3,7,7,11-tetra-methyl-10-aza-tetra-cyclo-[6.5.0.0(1,3).0(9,11)]trideca-ne.
Acta Crystallogr Sect E Struct Rep Online. 2013 Mar 28;69(Pt 4):o589-90. doi: 10.1107/S1600536813007642. Print 2013 Apr 1.
8
(1S,3R,8R,11S)-11-Bromo-10-bromo-methyl-2,2-di-chloro-3,7,7-tri-methyl-tricyclo-[6.4.0.0(1,3)]dodec-9-ene.
Acta Crystallogr Sect E Struct Rep Online. 2013 Jul 20;69(Pt 8):o1283. doi: 10.1107/S1600536813019697. eCollection 2013.
9
(1S,3R,8R)-2,2-Di-chloro-3,7,7,10-tetra-methyl-tri-cyclo-[6.4.0.0(1,3)]dodec-9-en-11-one.
Acta Crystallogr Sect E Struct Rep Online. 2013 May 4;69(Pt 6):o830. doi: 10.1107/S1600536813011781. Print 2013 Jun 1.
10
(1S,2R,7R,8S,10R)-9,9-Di-bromo-2,6,6,10-tetra-methyl-1α,2α-ep-oxy-tri-cyclo-[5.5.0.0(8,10)]dodeca-ne.
Acta Crystallogr Sect E Struct Rep Online. 2013 Jun 8;69(Pt 7):o1037-8. doi: 10.1107/S160053681301502X. eCollection 2013.

本文引用的文献

1
2,2-Dichloro-3,7,7,11-tetra-methyl-10-aza-tetra-cyclo-[6.5.0.0(1,3).0(9,11)]trideca-ne.
Acta Crystallogr Sect E Struct Rep Online. 2013 Mar 28;69(Pt 4):o589-90. doi: 10.1107/S1600536813007642. Print 2013 Apr 1.
2
(1S,3R,8R,9R,10S)-2,2-Dibromo-3,7,7,10-tetra-methyl-9β,10β-ep-oxy-3,7,7,10-tetra-methyl-tricyclo-[6.4.0.0(1,3)]dodeca-ne.
Acta Crystallogr Sect E Struct Rep Online. 2013 Mar 9;69(Pt 4):o521-2. doi: 10.1107/S1600536813006077. Print 2013 Apr 1.
3
(1S,3R,8R,9S,11R)-2,2,10,10-Tetra-chloro-3,7,7,11-tetra-methyl-tetra-cyclo-[6.5.0.0(1,3).0(9,11)]trideca-ne.
Acta Crystallogr Sect E Struct Rep Online. 2013 Feb 1;69(Pt 2):o275. doi: 10.1107/S1600536813001700. Epub 2013 Jan 23.
4
Structure validation in chemical crystallography.
Acta Crystallogr D Biol Crystallogr. 2009 Feb;65(Pt 2):148-55. doi: 10.1107/S090744490804362X. Epub 2009 Jan 20.
5
A short history of SHELX.
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.

文献AI研究员

20分钟写一篇综述,助力文献阅读效率提升50倍。

立即体验

用中文搜PubMed

大模型驱动的PubMed中文搜索引擎

马上搜索

文档翻译

学术文献翻译模型,支持多种主流文档格式。

立即体验