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纤维增强复合材料桩的成分和表面处理对与复合树脂粘结强度的影响。

Effect of components and surface treatments of fiber-reinforced composite posts on bond strength to composite resin.

机构信息

Advanced Biomaterials, Department of Restorative Sciences, Division of Oral Health Sciences, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University, 1-5-45 Yushima, Bunkyo-ku, Tokyo 113-8549, Japan.

出版信息

J Mech Behav Biomed Mater. 2013 Oct;26:23-33. doi: 10.1016/j.jmbbm.2013.05.022. Epub 2013 May 30.

Abstract

The aim of this study was to clarify the effect of the components and surface treatments of fiber-reinforced composite (FRC) posts on the durable bonding to core build-up resin evaluated using the pull-out and microtensile tests. Four types of experimental FRC posts, combinations of two types of matrix resins (polymethyl methacrylate and urethane dimethacrylate) and two types of fiberglass (E-glass and zirconia-containing glass) were examined. The FRC posts were subjected to one of three surface treatments (cleaned with ethanol, dichloromethane, or sandblasting). The bond strength between the FRC posts and core build-up resin were measured using the pull-out and microtensile tests before and after thermal cycling. The bond strengths obtained by each test before and after thermal cycling were statistically analyzed by three-way ANOVA and Tukey's multiple comparisons test (p<0.05). The bond strengths except for UDMA by the pull-out test decreased after thermal cycling. Regardless the test method and thermal cycling, matrix resins, the surface treatment and their interaction were statistically significant, but fiberglass did not. Dichloromethane treatment was effective for the PMMA-based FRC posts by the pull-out test, but not by the microtensile test. Sandblasting was effective for both PMMA- and UDMA-based FRC posts, regardless of the test method. The bond strengths were influenced by the matrix resin of the FRC post and the surface treatment. The bond strengths of the pull-out test showed a similar tendency of those of the microtensile test, but the value obtained by these test were different.

摘要

本研究旨在阐明纤维增强复合材料(FRC)桩的成分和表面处理对使用拔出和微拉伸试验评估的核树脂耐用粘结的影响。研究了四种实验性 FRC 桩,它们由两种基质树脂(聚甲基丙烯酸甲酯和聚氨酯二甲基丙烯酸酯)和两种玻璃纤维(E 玻璃和含氧化锆玻璃)组合而成。对 FRC 桩进行了三种表面处理之一(用乙醇、二氯甲烷或喷砂清洗)。在热循环前后,使用拔出和微拉伸试验测量 FRC 桩和核树脂之间的粘结强度。通过三因素方差分析和 Tukey 多重比较检验(p<0.05)对热循环前后每种试验获得的粘结强度进行统计学分析。热循环后,除了拔出试验中的 UDMA 之外,所有试验的粘结强度均降低。无论试验方法和热循环如何,基质树脂、表面处理及其相互作用均具有统计学意义,但玻璃纤维没有。对于基于 PMMA 的 FRC 桩,二氯甲烷处理在拔出试验中有效,但在微拉伸试验中无效。喷砂处理对基于 PMMA 和 UDMA 的 FRC 桩均有效,无论试验方法如何。粘结强度受 FRC 桩的基质树脂和表面处理的影响。拔出试验的粘结强度与微拉伸试验的粘结强度具有相似的趋势,但这些试验的结果值不同。

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