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复合树脂耐磨性和硬度的体外研究。

An in vitro investigation of wear resistance and hardness of composite resins.

作者信息

Cao Liqun, Zhao Xinyi, Gong Xu, Zhao Shouliang

机构信息

School of Stomatology, Tongji University Shanghai 200072, China.

出版信息

Int J Clin Exp Med. 2013 Jun 26;6(6):423-30. Print 2013.

Abstract

PURPOSE

The aim of the present study was to investigate the wear resistance and hardness of five kinds of composite resins.

MATERIALS AND METHODS

Sixty-five specimens were fabricated with one nano-hybrid (Charisma Diamond), two micro-hybrid (3MZ250, Clearfil AP-X) and two packable (3MP60, Surefil) composite resins, according to a randomized complete block design (n=13, 8 for wear test; 5 for hardness test). The composites were filled in a rectangular mold, and light polymerization. After storage in 37°C deionized water for 24h, all specimens were tested with a custom-made toothbrush machine with a stainless-steel ball as antagonist (3N loads, 1Hz, 6×10(5) cycles) immersed in calcium fluoride slurry. Wear volume, hardness and surface structure of each tested material was examined by a three-dimensional non-contact optical profilometer, Vickers indentation technique and scanning electron microscope.

RESULTS

The volume loss ranked from least to most as follows: Charisma Diamond, P60, Z250, Clearfil AP-X and Surefil. Regarding hardness, the rank from highest to lowest as follows: Clearfil AP-X, P60, Surefil, Z250, Charisma Diamond. The interactions between wear resistance and microhardness were not significant.

CONCLUSIONS

The custom-made machine is considered suitable to simulate sliding of an antagonist cusp on an opposing occlusal composite restoration. Nanofilled composite may have superior wear compared to other composite resins.

摘要

目的

本研究旨在调查五种复合树脂的耐磨性和硬度。

材料与方法

根据随机完全区组设计(n = 13,8个用于磨损试验;5个用于硬度试验),用一种纳米混合复合树脂(魅力钻石)、两种微混合复合树脂(3MZ250、Clearfil AP-X)和两种可压实复合树脂(3MP60、Surefil)制作65个样本。将复合材料填充到矩形模具中,并进行光聚合。在37°C去离子水中储存24小时后,所有样本在一台定制的牙刷试验机上进行测试,该试验机以不锈钢球作为拮抗剂(3N载荷,1Hz,6×10⁵次循环),样本浸在氟化钙浆液中。通过三维非接触光学轮廓仪、维氏压痕技术和扫描电子显微镜检查每种测试材料的磨损体积、硬度和表面结构。

结果

磨损体积从最小到最大的排序如下:魅力钻石、P60、Z250、Clearfil AP-X和Surefil。关于硬度,从最高到最低的排序如下:Clearfil AP-X、P60、Surefil、Z250、魅力钻石。耐磨性和显微硬度之间的相互作用不显著。

结论

该定制机器被认为适合模拟拮抗剂牙尖在相对的咬合复合修复体上的滑动。与其他复合树脂相比,纳米填充复合树脂可能具有更好的耐磨性。

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