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机械和热负荷循环对Clearfil SE粘结剂与表层牙本质微拉伸粘结强度的影响。

Effects of mechanical and thermal load cycling on micro tensile bond strength of clearfil SE bond to superficial dentin.

作者信息

Daneshkazemi Ali Reza, Davari Abdol Rahim, Ataei Ebrahim, Dastjerdi Fariba, Hajighasemi Ehsan

机构信息

Department of Operative Dentistry, Member of Social Determinants of Oral Health Research Center, Yazd, Iran.

出版信息

Dent Res J (Isfahan). 2013 Mar;10(2):202-9. doi: 10.4103/1735-3327.113344.

Abstract

BACKGROUND

Certain studies have been conducted on the effects of mechanical and thermal load cycling on the microtensile bond strength (microTBS) of composites to dentin, but the results were different. The authors therefore decided to evaluate these effects on the bonding of Clearfil SE bond to superficial dentin.

MATERIALS AND METHODS

Flat dentinal surface of 42 molar teeth were bonded to Filtek-Z250 resin composite by Clearfil SE bond. The teeth were randomly divided into 7 groups and exposed to different mechanical and thermal load cycling. Thermocycling was at 5-55°C and mechanical load cycling was created with a force of 125 N and 0.5 Hz. Then, the teeth were sectioned and shaped to hour glass form and subjected to microTBS testing at a speed of 0.5 mm/min. The results were statistically analyzed by computer with three-way analysis of variance and T-test at P < 0.05 significant. To evaluate the location and mode of failure, the specimens were observed under the stereomicroscope. Then, one of the specimens in each group was evaluated under Scanning Electron Microscopy (SEM) for mode of failure.

RESULTS

All of the study groups had a significantly lower microTBS as compared to the control group (P < 0.001). There was no statistically significant difference between mechanical cycling with 50K (kilo = 1000) cycles, and 50K mechanical cycles plus 1K thermal cycles. Most of the fractures in the control group were of adhesive type and this type of fracture increased after exposure to mechanical and thermal load cycling.

CONCLUSION

Thermal and mechanical load cycling had significant negative effects on microTBS and the significant effects of mechanical load cycling started to be significant at 100K cycles.

摘要

背景

已经进行了一些关于机械和热循环加载对复合材料与牙本质的微拉伸粘结强度(microTBS)影响的研究,但结果各不相同。因此,作者决定评估这些因素对Clearfil SE粘结剂与表层牙本质粘结的影响。

材料与方法

用Clearfil SE粘结剂将42颗磨牙的平坦牙本质表面粘结到Filtek-Z250树脂复合材料上。将牙齿随机分为7组,使其承受不同的机械和热循环加载。热循环温度为5-55°C,机械循环加载力为125 N,频率为0.5 Hz。然后,将牙齿切片并加工成沙漏形状,以0.5 mm/min的速度进行微拉伸粘结强度测试。结果采用计算机进行统计分析,采用三因素方差分析和T检验,P<0.05为有统计学意义。为了评估断裂位置和模式,在体视显微镜下观察标本。然后,每组中的一个标本在扫描电子显微镜(SEM)下评估断裂模式。

结果

与对照组相比,所有研究组的微拉伸粘结强度均显著降低(P<0.001)。50K(千=1000)次机械循环组与50K次机械循环加1K次热循环组之间无统计学显著差异。对照组中的大多数断裂为粘结型,在承受机械和热循环加载后,这种断裂类型增加。

结论

热循环和机械循环加载对微拉伸粘结强度有显著负面影响,机械循环加载的显著影响在100K次循环时开始显现。

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