J Adhes Dent. 2014 Feb;16(1):7-14. doi: 10.3290/j.jad.a30554.
This study compared the microtensile bond strengths (μTBS) of two different self-etching (SE) and etchand- rinse (ER) adhesive systems to enamel affected by hypoplastic amelogenesis imperfecta (HPAI) and analyzed the enamel etching patterns created by the two adhesive systems using scanning electron microscopy (SEM).
Sixteen extracted HPAI-affected molars were used for the bond strength tests and 2 molars were examined under SEM for etching patterns. The control groups consisted of 12 healthy third molars for μTBS tests and two molars for SEM. Mesial and distal surfaces of the teeth were slightly ground flat. The adhesive systems and composite resin were applied to the flat enamel surfaces according to the manufacturers' instructions. The tooth slabs containing composite resin material on their mesial and distal surfaces were cut in the mesio-distal direction with a slow-speed diamond saw. The slabs were cut again to obtain square, 1-mm-thick sticks. Finally, each stick was divided into halves and placed in the μTBS tester. Bond strength tests were performed at a speed of 0.5 mm/min. Data were analyzed with two-way ANOVA and Tukey's tests.
There was no significant difference between the bond strength values of ER and SE adhesives (p > 0.05). However, significant differences were found between HPAI and control groups (p < 0.05). HPAI-affected enamel surfaces exhibited mild intra- and inter-prismatic enamel etching patterns after orthophosphoric acid application, while conditioning of HPAI-affected enamel with SE primer created a slightly rough and grooved surface.
SE and ER adhesive systems provide similar bond strengths to HPAI-affected enamel surfaces.
本研究比较了两种不同的自酸蚀(SE)和酸蚀-冲洗(ER)粘接系统对牙釉质发育不全型(HPAI)牙釉质的微拉伸粘接强度(μTBS),并采用扫描电子显微镜(SEM)分析了两种粘接系统对牙釉质的蚀刻模式。
16 颗 HPAI 受累磨牙用于粘接强度测试,2 颗磨牙用于 SEM 蚀刻模式检查。对照组包括 12 颗健康第三磨牙用于 μTBS 测试和 2 颗磨牙用于 SEM。牙齿的近中和远中表面稍微磨平。根据制造商的说明,将粘接系统和复合树脂应用于平坦的牙釉质表面。在近远中方向上,用低速金刚石锯将含有复合树脂材料的牙面切割成薄片。然后再次切割薄片,以获得 1mm 厚的方形小棒。最后,将每个小棒分成两半,并放入 μTBS 测试仪中。以 0.5mm/min 的速度进行粘接强度测试。采用双因素方差分析和 Tukey 检验对数据进行分析。
ER 和 SE 粘接剂的粘接强度值之间无显著差异(p>0.05)。然而,HPAI 组与对照组之间存在显著差异(p<0.05)。应用磷酸后,HPAI 牙釉质表面呈现轻度的内、间柱牙釉质蚀刻模式,而 SE 底漆处理 HPAI 牙釉质则形成略微粗糙和有凹槽的表面。
SE 和 ER 粘接系统对 HPAI 受累牙釉质表面提供相似的粘接强度。