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利用电子鼻对农业馏分进行质量评估。

Quality evaluation of agricultural distillates using an electronic nose.

机构信息

Department of Analytical Chemistry, Chemical Faculty, Gdansk University of Technology, 11/12 G. Narutowicza Str., 80-233 Gdańsk, Poland.

出版信息

Sensors (Basel). 2013 Nov 25;13(12):15954-67. doi: 10.3390/s131215954.

Abstract

The paper presents the application of an electronic nose instrument to fast evaluation of agricultural distillates differing in quality. The investigations were carried out using a prototype of electronic nose equipped with a set of six semiconductor sensors by FIGARO Co., an electronic circuit converting signal into digital form and a set of thermostats able to provide gradient temperature characteristics to a gas mixture. A volatile fraction of the agricultural distillate samples differing in quality was obtained by barbotage. Interpretation of the results involved three data analysis techniques: principal component analysis, single-linkage cluster analysis and cluster analysis with spheres method. The investigations prove the usefulness of the presented technique in the quality control of agricultural distillates. Optimum measurements conditions were also defined, including volumetric flow rate of carrier gas (15 L/h), thermostat temperature during the barbotage process (15 °C) and time of sensor signal acquisition from the onset of the barbotage process (60 s).

摘要

本文介绍了一种电子鼻仪器在快速评估质量不同的农业馏分中的应用。该研究使用了配备由 FIGARO 公司生产的六组半导体传感器的电子鼻原型、将信号转换为数字形式的电子电路以及一组能够为气体混合物提供梯度温度特性的恒温器进行。通过鼓泡法获得了挥发性馏分样品,这些样品的质量不同。结果的解释涉及三种数据分析技术:主成分分析、单链接聚类分析和聚类分析与球体方法。研究证明了所提出的技术在农业馏分质量控制中的有用性。还定义了最佳测量条件,包括载气的体积流量(15 L/h)、鼓泡过程中的恒温器温度(15°C)以及从鼓泡过程开始传感器信号采集的时间(60 s)。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d74e/3892867/a263b1ce8884/sensors-13-15954f1.jpg

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