[广东紫珠不同产地及部位中连翘酯苷B和紫珠苷的测定]

[Determination of forsythiaside B and poliumoside in different origin and parts from Callicarpa kwangtungensis].

作者信息

Liu Can-Huang, Liu Ta-Si, Luo Chen-Qu, Zhang Ji, Zeng Xiao-Yan, Cui Lei, Xie Li-Juan

机构信息

Hunan University of Traditional Chinese Medicine, Changsha 410208, China.

Institute for Drug and Food Contrl of Loudi, Loudi 417000, China.

出版信息

Zhongguo Zhong Yao Za Zhi. 2013 Oct;38(19):3324-6.

PMID:24422401

Abstract

The RP-HPLC method was used to determinate the contents of forsythiaside B and poliumoside in different origin and parts from Callicarpa kwangtungensis. The linear ranges of forsythiaside B and poliumoside were 0. 106-3. 18 and 0. 105 2-3. 156 microg, respectively. The average recoveries of forythiaside B and poliumoside were 99. 01% ( RSD 1. 2%) and 100. 13% (RSD 0. 90% ), respectively. The contents of forsythiaside B and poliumoside were changed in different origin and parts from C. kwangtungensis. The sample from the area of Luxi, Pingxiang City, Jiangxi Province has the highest contents of forsythiaside B and poliumoside. The contents of forsythiaside B and poliumoside in different parts from C. kwangtungensis in Luxi are: leaf > stem > fruit. This result will provide a scientific basis for quality control and reasonable utilzation of C. kwangtungensis.

摘要

采用反相高效液相色谱法测定广东紫珠不同产地及部位中连翘酯苷B和紫珠苷的含量。连翘酯苷B和紫珠苷的线性范围分别为0.106 - 3.18 μg和0.105 2 - 3.156 μg。连翘酯苷B和紫珠苷的平均回收率分别为99.01%（RSD 1.2%）和100.13%（RSD 0.90%）。广东紫珠不同产地及部位中连翘酯苷B和紫珠苷的含量存在差异。江西省萍乡市芦溪地区的样品中连翘酯苷B和紫珠苷含量最高。芦溪广东紫珠不同部位中连翘酯苷B和紫珠苷的含量为：叶＞茎＞果实。该结果将为广东紫珠的质量控制和合理利用提供科学依据。