Nayak Prakash S, Narayana B, Jasinski Jerry P, Yathirajan H S, Kaur Manpreet
Department of Studies in Chemistry, Mangalore University, Mangalagangotri 574 199, India.
Department of Chemistry, Keene State College, 229 Main Street, Keene, NH 03435-2001, USA.
Acta Crystallogr Sect E Struct Rep Online. 2013 Oct 9;69(Pt 11):o1622. doi: 10.1107/S160053681302730X.
The title compound, C9H8N2OS, crystallizes with two mol-ecules (A and B) in the asymmetric unit. The dihedral angles between the mean planes of the 1,3-benzo-thia-zol-2-yl ring system and the acetamide group are 2.7 (4) (mol-ecule A) and 7.2 (2) Å (mol-ecule B). In the crystal, pairs of N-H⋯N hydrogen bonds link the A and B mol-ecules into dimers, generating R 2 (2)(8) loops. The dimers stack along [100].
标题化合物C9H8N2OS在不对称单元中由两个分子(A和B)结晶而成。1,3 - 苯并噻唑 - 2 - 基环系统的平均平面与乙酰胺基团之间的二面角分别为2.7(4)°(分子A)和7.2(2)°(分子B)。在晶体中,N - H⋯N氢键对将A和B分子连接成二聚体,形成R2(2)(8)环。二聚体沿[100]方向堆积。