采用超高效液相色谱-质谱联用技术对蜂蜜中的兽药进行全面筛查。
Comprehensive screening of veterinary drugs in honey by ultra-high-performance liquid chromatography coupled to mass spectrometry.
作者信息
Staub Spörri Aline, Jan Philippe, Cognard Emmanuelle, Ortelli Didier, Edder Patrick
机构信息
a Official Food Control Authority and Veterinary Affairs of Geneva , 22 Quai Ernest-Ansermet, 1211 Geneva 4, Switzerland.
出版信息
Food Addit Contam Part A Chem Anal Control Expo Risk Assess. 2014;31(5):806-16. doi: 10.1080/19440049.2014.891295. Epub 2014 Apr 7.
In the context of multi-residue screening in honey, a complete methodology was developed for 200 veterinary drugs comprising a sample preparation step and an ultra-high-performance liquid chromatography (UHPLC) coupled to time-of-flight (TOF) mass spectrometry analysis. In addition, specific analytical strategies were developed for two compounds, streptomycin and chloramphenicol, using UHPLC and tandem mass spectrometry (MS/MS). Methodologies were then applied to real honey samples obtained from the Swiss market.
在蜂蜜多残留筛查的背景下，开发了一种针对200种兽药的完整方法，该方法包括样品制备步骤以及超高效液相色谱（UHPLC）与飞行时间（TOF）质谱联用分析。此外，还使用UHPLC和串联质谱（MS/MS）为链霉素和氯霉素这两种化合物开发了特定的分析策略。然后将这些方法应用于从瑞士市场获取的真实蜂蜜样品。
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