Lippmann M, Ehnes A, Seeck O H
Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany.
Rev Sci Instrum. 2014 Jan;85(1):015106. doi: 10.1063/1.4860057.
A setup has been designed to investigate thin films of confined liquids with the use of X-ray scattering methods. The confinement is realized between the flat culets of a pair of diamonds by positioning and orienting the lower diamond with nanometer and micro radian accuracy. We routinely achieve gaps between 5 and 50 nm at culet diameters of 200 μm. With this setup and a micro focused X-ray beam we have investigated the in-plane and the out-off-plane atomic order of benzene with atomic resolution.
已设计出一种装置，用于利用X射线散射方法研究受限液体的薄膜。通过以纳米和微弧度精度定位和定向下部钻石，在一对钻石的平面小面之间实现限制。在200μm的小面直径下，我们通常能实现5至50nm的间隙。利用该装置和微聚焦X射线束，我们以原子分辨率研究了苯的面内和面外原子排列。
