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热机械老化对用自酸蚀粘结剂和自粘结树脂水门汀粘结到天然牙上的玻璃纤维桩和氧化锆桩的粘结强度及界面形态的影响。

Effect of thermomechanical aging on bond strength and interface morphology of glass fiber and zirconia posts bonded with a self-etch adhesive and a self-adhesive resin cement to natural teeth.

作者信息

Yaman Batu Can, Ozer Fusun, Takeichi Takuro, Karabucak Bekir, Koray Fatma, Blatz Markus B

机构信息

Associate Professor, Istanbul University, Faculty of Dentistry, Department of Operative Dentistry, Eskişehir, Turkey.

Professor, Department of Preventive and Restorative Sciences, University of Pennsylvania School of Dental Medicine, Philadelphia, Pa.

出版信息

J Prosthet Dent. 2014 Sep;112(3):455-64. doi: 10.1016/j.prosdent.2013.11.008. Epub 2014 Mar 28.

Abstract

STATEMENT OF PROBLEM

Information regarding the effect of thermomechanical aging (TMA) on the bond strength of luting cements to root canal dentin and endodontic posts is limited.

PURPOSE

The purpose of this study was to investigate the effect of TMA on the bond strength of fiber and zirconia posts bonded to root canal dentin with 2 different resin cements with microtensile and scanning electron microscopic evaluation.

MATERIAL AND METHODS

Eighty extracted single-rooted human premolars were endodontically treated and restored with either a glass fiber post (FP) or a zirconia post (ZP) with 2 commercially available resin luting cements. The teeth were divided into 2 main groups. In the first group, posts (n=40) were bonded with a self-etch adhesive cement (SEAC). In the second group (n=40), posts were bonded using a self-adhesive cement (SAC). During the first aging phase, all specimens in each group were stored in distilled water for 30 days at 37°C. During the second phase, half of the specimens in each group were subjected to the TMA. The test groups were as follows: FP/SEAC, FP/SEAC+TMA, ZP/SEAC, ZP/SEAC+TMA, FP/SAC, FP/SAC+TMA, ZP/SAC, and ZP/SAC+TMA. The bond strength was measured with a microtensile test. Data were analyzed by 3-way analysis of variance and the Tukey honest significant different test (α=.05).

RESULTS

FP/SEAC at 30 days was higher than in the other groups. However, bond strength values were significantly reduced in this group after TMA (P<.001).

CONCLUSIONS

Bond strength values and physical properties of SEAC with higher filler content were more affected by the TMA than those of SALC. According to scanning electron microscopic observation, TMA also affected the micromorphologic interface between the posts and the resin cements as well as between the resin cements and the root canal dentin.

摘要

问题陈述

关于热机械老化(TMA)对粘结水门汀与根管牙本质及根管桩粘结强度影响的信息有限。

目的

本研究旨在通过微拉伸和扫描电子显微镜评估,研究TMA对用两种不同树脂水门汀粘结至根管牙本质的纤维桩和氧化锆桩粘结强度的影响。

材料与方法

80颗拔除的单根人前磨牙经根管治疗后,用两种市售树脂粘结水门汀分别与玻璃纤维桩(FP)或氧化锆桩(ZP)进行修复。牙齿分为两个主要组。第一组,40颗桩用自酸蚀粘结水门汀(SEAC)粘结。第二组(40颗),桩用自粘结水门汀(SAC)粘结。在第一个老化阶段,每组所有标本在37°C蒸馏水中储存30天。在第二阶段,每组一半标本进行TMA处理。试验组如下:FP/SEAC、FP/SEAC+TMA、ZP/SEAC、ZP/SEAC+TMA、FP/SAC、FP/SAC+TMA、ZP/SAC和ZP/SAC+TMA。用微拉伸试验测量粘结强度。数据通过三因素方差分析和Tukey真实显著性差异检验进行分析(α=0.05)。

结果

30天时FP/SEAC组高于其他组。然而,该组在TMA处理后粘结强度值显著降低(P<0.001)。

结论

填料含量较高的SEAC的粘结强度值和物理性能比SALC受TMA的影响更大。根据扫描电子显微镜观察,TMA还影响了桩与树脂水门汀之间以及树脂水门汀与根管牙本质之间的微观形态界面。

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