Gong Xiao-Mei, Wang Shuo, Zhou Xiao-Lei, Zhou Dan-Dan, Dai Hang, Deng Jia-Gang
Zhong Yao Cai. 2013 Oct;36(10):1614-6.
To study the chemical constituents of ethyl acetate fraction of Citrullus vulgaris Schrad vine.
Compounds were isolated and purified by polyamide column chromatography, silica gel column chromatography, thin layer chromatography and sephadex gel column chromatography. Their structures were elucidated on the basis of physicochemical properties and spectral data.
Ten compounds were isolated from Citrullus vulgaris Schrad vine and elucidated as: pentadecanoic acid (1), monopentadecanoin (2), 2, 3-dihydroxypropyl nonadecoate (3), lignoceric acid-2, 3-dihydroxy-propanenyl ester (4), lancerebroside 5 (5), salicylic acid (6), 4-hydroxybenzoic acid (7), hydroquinone (8), succinic acid (9) and vanillic acid (10).
Compounds 1 - 10 are obtained from Citrullus vulgaris Schrad vine for the first time.
研究西瓜藤乙酸乙酯部位的化学成分。
采用聚酰胺柱色谱、硅胶柱色谱、薄层色谱和葡聚糖凝胶柱色谱对化合物进行分离纯化,并根据理化性质和光谱数据对其结构进行鉴定。
从西瓜藤中分离得到10个化合物,分别鉴定为:十五烷酸(1)、单十五烷甘油酯(2)、2,3 - 二羟基丙基十九烷酸酯(3)、木蜡酸 - 2,3 - 二羟基丙酯(4)、披针叶黄华苷5(5)、水杨酸(6)、4 - 羟基苯甲酸(7)、对苯二酚(8)、琥珀酸(9)和香草酸(10)。
化合物1 - 10首次从西瓜藤中获得。