Wernecke Jan, Gollwitzer Christian, Müller Peter, Krumrey Michael
Physikalisch-Technische Bundesanstalt (PTB), Abbestrasse 2-12, 10587 Berlin, Germany.
J Synchrotron Radiat. 2014 May;21(Pt 3):529-36. doi: 10.1107/S160057751400294X. Epub 2014 Mar 13.
A dedicated in-vacuum X-ray detector based on the hybrid pixel PILATUS 1M detector has been installed at the four-crystal monochromator beamline of the PTB at the electron storage ring BESSY II in Berlin, Germany. Owing to its windowless operation, the detector can be used in the entire photon energy range of the beamline from 10 keV down to 1.75 keV for small-angle X-ray scattering (SAXS) experiments and anomalous SAXS at absorption edges of light elements. The radiometric and geometric properties of the detector such as quantum efficiency, pixel pitch and module alignment have been determined with low uncertainties. The first grazing-incidence SAXS results demonstrate the superior resolution in momentum transfer achievable at low photon energies.
基于混合像素PILATUS 1M探测器的专用真空X射线探测器已安装在德国柏林电子储存环BESSY II的PTB四晶单色仪光束线上。由于其无窗操作,该探测器可用于光束线的整个光子能量范围,从10 keV到1.75 keV,用于小角X射线散射(SAXS)实验和轻元素吸收边缘处的反常SAXS。探测器的辐射和几何特性,如量子效率、像素间距和模块对准,已在低不确定性下确定。首次掠入射SAXS结果表明,在低光子能量下可实现卓越的动量转移分辨率。