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N-（3-氯-1-甲基-1H-吲唑-5-基）-4-甲基苯磺酰胺

N-(3-Chloro-1-methyl-1H-indazol-5-yl)-4-methylbenzene-sulfonamide.

作者信息

Chicha Hakima, Rakib El Mostapha, Amiri Ouafa, Saadi Mohamed, El Ammari Lahcen

机构信息

Laboratoire de Chimie Organique et Analytique, Université Sultan Moulay Slimane, Faculté des Sciences et Techniques, Béni-Mellal, BP 523, Morocco.

Laboratoire de Chimie du Solide Appliquée, Faculté des Sciences, Université Mohammed V-Agdal, Avenue Ibn Battouta, BP 1014, Rabat, Morocco.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2014 Jan 22;70(Pt 2):o181. doi: 10.1107/S1600536814001184. eCollection 2014 Feb 1.

DOI:10.1107/S1600536814001184
PMID:24764895
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3998334/
Abstract

The asymmetric unit of the title compound, C15H14ClN3O2S, contains two independent mol-ecules showing different conformations: in one mol-ecule, the indazole ring system makes a dihedral angle of 51.5 (1)° with the benzene ring whereas in the other, the indazole unit is almost perpendicular to the benzene ring [dihedral angle 77.7 (1)°]. In the crystal, the mol-ecules are linked by N-H⋯N and N-H⋯O hydrogen bonds, forming a set of four mol-ecules linked in pairs about an inversion centre.

摘要

标题化合物C₁₅H₁₄ClN₃O₂S的不对称单元包含两个呈现不同构象的独立分子：在一个分子中，吲唑环系统与苯环的二面角为51.5 (1)°，而在另一个分子中，吲唑单元几乎垂直于苯环[二面角77.7 (1)°]。在晶体中，分子通过N-H⋯N和N-H⋯O氢键相连，形成一组围绕一个反演中心成对相连的四个分子。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3930/3998334/c3914abbc18d/e-70-0o181-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3930/3998334/56862f9fbdb2/e-70-0o181-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3930/3998334/c3914abbc18d/e-70-0o181-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3930/3998334/56862f9fbdb2/e-70-0o181-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3930/3998334/c3914abbc18d/e-70-0o181-fig2.jpg

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