Freifrau Von Maltzahn Nadine, Kleibe Martin, Stiesch Meike, Hübsch Christoph, Kohorst Philipp
Department of Prosthetic Dentistry and Biomedical Materials Science, Hannover Medical School.
Dent Mater J. 2014;33(5):583-90. doi: 10.4012/dmj.2013-181. Epub 2014 Apr 29.
The aim of this study was to investigate how changes in the thermal characteristics of veneer ceramics with almost identical chemical and mechanical properties but with different coefficients of thermal expansion (CTE) can modify their interfacial adhesion to zirconia. 48 bilayers made of one Y-TZP ceramic and four veneer ceramics were fabricated (n=12). Thermal residual stresses were calculated on the basis of the CTE and glass transition temperatures. After defined notching all specimens were loaded in a four-point bending test and the critical loads were recorded which induced stable crack extension at the adhesion interface. The strain energy release rate (G, J/m(2)) was calculated and was taken as a measure of interfacial adhesion. The CTE of the veneer ceramics were significantly correlated with their adhesion to Y-TZP (p<0.001). Interfacial adhesion in zirconia/veneer bilayers is predominantly affected by the thermal characteristics of the veneer ceramic.
本研究的目的是调查具有几乎相同化学和机械性能但热膨胀系数(CTE)不同的饰面陶瓷的热特性变化如何改变它们与氧化锆的界面附着力。制备了由一种Y-TZP陶瓷和四种饰面陶瓷组成的48个双层结构(n = 12)。基于CTE和玻璃化转变温度计算热残余应力。在进行特定刻痕后,所有试样在四点弯曲试验中加载,并记录在粘结界面处引起稳定裂纹扩展的临界载荷。计算应变能释放率(G,J/m²),并将其作为界面附着力的度量。饰面陶瓷的CTE与其与Y-TZP的附着力显著相关(p<0.001)。氧化锆/饰面双层结构中的界面附着力主要受饰面陶瓷热特性的影响。