Two-dimensional NMR spectroscopy with temperature-sweep.
作者信息
Bermel Wolfgang, Dass Rupashree, Neidig Klaus-Peter, Kazimierczuk Krzysztof
机构信息
Bruker BioSpin GmbH, Silberstreifen, 76287 Rheinstetten (Germany).
出版信息
Chemphyschem. 2014 Aug 4;15(11):2217-20. doi: 10.1002/cphc.201402191. Epub 2014 May 26.
PMID:24863674
Abstract
Two-dimensional nuclear magnetic resonance (NMR) spectroscopy is useful for studying temperature-dependent effects on molecular structure. However, experimental time is usually long, because sampling is repeated at several temperatures. A novel solution to the problem is proposed, in which signal sampling is performed in parallel to the linear temperature-sweep.
摘要
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