Lee Koon-Yang, Shamsuddin Siti Rosminah, Fortea-Verdejo Marta, Bismarck Alexander
Polymer and Composite Engineering (PaCE) Group, Institute of Materials Chemistry and Research, University of Vienna; Department of Chemical Engineering, University College London;
Polymer and Composite Engineering (PaCE) Group, Department of Chemical Engineering, Imperial College London.
J Vis Exp. 2014 May 22(87):51432. doi: 10.3791/51432.
A novel method of manufacturing rigid and robust natural fiber preforms is presented here. This method is based on a papermaking process, whereby loose and short sisal fibers are dispersed into a water suspension containing bacterial cellulose. The fiber and nanocellulose suspension is then filtered (using vacuum or gravity) and the wet filter cake pressed to squeeze out any excess water, followed by a drying step. This will result in the hornification of the bacterial cellulose network, holding the loose natural fibers together. Our method is specially suited for the manufacturing of rigid and robust preforms of hydrophilic fibers. The porous and hydrophilic nature of such fibers results in significant water uptake, drawing in the bacterial cellulose dispersed in the suspension. The bacterial cellulose will then be filtered against the surface of these fibers, forming a bacterial cellulose coating. When the loose fiber-bacterial cellulose suspension is filtered and dried, the adjacent bacterial cellulose forms a network and hornified to hold the otherwise loose fibers together. The introduction of bacterial cellulose into the preform resulted in a significant increase of the mechanical properties of the fiber preforms. This can be attributed to the high stiffness and strength of the bacterial cellulose network. With this preform, renewable high performance hierarchical composites can also be manufactured by using conventional composite production methods, such as resin film infusion (RFI) or resin transfer molding (RTM). Here, we also describe the manufacturing of renewable hierarchical composites using double bag vacuum assisted resin infusion.
本文介绍了一种制造刚性且坚固的天然纤维预制件的新方法。该方法基于造纸工艺,将松散的短剑麻纤维分散到含有细菌纤维素的水悬浮液中。然后对纤维和纳米纤维素悬浮液进行过滤(使用真空或重力),并对湿滤饼进行压制以挤出多余的水分,随后进行干燥步骤。这将导致细菌纤维素网络角质化,从而将松散的天然纤维固定在一起。我们的方法特别适用于制造亲水性纤维的刚性且坚固的预制件。此类纤维的多孔和亲水性导致大量吸水,从而吸入悬浮液中分散的细菌纤维素。然后细菌纤维素会附着在这些纤维表面进行过滤,形成细菌纤维素涂层。当松散的纤维 - 细菌纤维素悬浮液经过过滤和干燥后,相邻的细菌纤维素形成网络并角质化,将原本松散的纤维固定在一起。在预制件中引入细菌纤维素可显著提高纤维预制件的机械性能。这可归因于细菌纤维素网络的高刚度和强度。利用这种预制件,还可以通过使用传统的复合材料生产方法,如树脂膜灌注(RFI)或树脂传递模塑(RTM)来制造可再生的高性能分级复合材料。在此处,我们还描述了使用双袋真空辅助树脂灌注制造可再生分级复合材料的过程。