Xu H H K, Schumacher G E, Eichmiller F C, Peterson R C, Antonucci J M, Mueller H J
Paffenbarger Research Center, National Institute of Standards and Technology, American Dental Association Health Foundation, 100 Bureau Drive Stop 8546, Gaithersburg, MD 20899-8546, USA.
Dent Mater. 2003 Sep;19(6):523-30. doi: 10.1016/s0109-5641(02)00100-8.
Direct-filling resin composites are used in relatively small restorations and are not recommended for large restorations with severe occlusal-stresses. The aim of this study was to reinforce composites with fiber preforms, and to investigate the effects of layer thickness and configurations on composite properties. It was hypothesized that fiber preforms would significantly increase the composite's flexural strength, work-of-fracture (toughness) and elastic modulus.
Glass fibers were silanized, impregnated with a resin, cured, and cut to form inserts for tooth cavity restorations. Also fabricated were three groups of specimens of 2mm x 2mm x 25 mm: a fiber preform rod in the center of a hybrid composite; a thin fiber layer on the tensile side of the specimens; and a thin fiber layer sandwiched in between layers of a hybrid composite. These specimens were tested in three-point flexure to measure strength, work-of-fracture and modulus. Optical and scanning electron microscopy were used to examine the restorations and the fiber distributions.
Microscopic examinations of insert-filled tooth cavities showed that the fibers were relatively uniform in distribution within the preform, and the inserts were well bonded with the surrounding hybrid composite. Specimens consisting of a fiber preform rod in the center of a hybrid composite had a flexural strength (mean (SD); n=6) of 313 (19)MPa, significantly higher than 120 (16)MPa of the hybrid composite without fibers (Tukey's at family confidence of 0.95). The work-of-fracture was increased by nearly seven times, and the modulus was doubled, due to fiber preform reinforcement. Similar improvements were obtained for the other two groups of specimens.
Substantial improvements in flexural strength, toughness and stiffness were achieved for dental resin composites reinforced with fiber preforms. The method of embedding a fiber preform insert imparts superior reinforcement to restorations and should improve the performance of direct-filling resin composites in large restorations with high occlusal-loads.
直接充填树脂复合材料用于相对较小的修复体,不推荐用于承受严重咬合应力的大型修复体。本研究的目的是用纤维预制件增强复合材料,并研究层厚和结构对复合材料性能的影响。假设纤维预制件会显著提高复合材料的弯曲强度、断裂功(韧性)和弹性模量。
对玻璃纤维进行硅烷化处理,用树脂浸渍,固化,然后切割成用于牙腔修复的嵌体。还制作了三组尺寸为2mm×2mm×25mm的试样:在混合复合材料中心放置一根纤维预制件棒;在试样的拉伸侧放置一层薄纤维;在混合复合材料层之间夹一层薄纤维。对这些试样进行三点弯曲试验,以测量强度、断裂功和模量。使用光学显微镜和扫描电子显微镜检查修复体和纤维分布。
对嵌体填充牙腔的显微镜检查表明,纤维在预制件内分布相对均匀,嵌体与周围的混合复合材料粘结良好。由混合复合材料中心的纤维预制件棒组成的试样的弯曲强度(平均值(标准差);n = 6)为313(19)MPa,显著高于无纤维混合复合材料的120(16)MPa(在家族置信度为0.95时进行Tukey检验)。由于纤维预制件的增强作用,断裂功增加了近7倍,模量增加了一倍。其他两组试样也有类似的改善。
用纤维预制件增强牙科树脂复合材料可显著提高其弯曲强度、韧性和刚度。嵌入纤维预制件嵌体的方法能为修复体提供优异的增强效果,并应能改善直接充填树脂复合材料在承受高咬合负荷的大型修复体中的性能。