Khoroushi Maryam, Rafizadeh Mojgan, Samimi Pouran
Associate Professor, Dental Materials Research Center and Department of of Operative Dentistry, School of Dentistry, Isfahan University of Medical Sciences, Isfahan, Iran.
Torabinejad Dental Research Center, School of Dentistry, Isfahan University of Medical Sciences, Isfahan, Iran.
J Dent (Tehran). 2014 Mar;11(2):150-60. Epub 2014 Mar 31.
Ethanol wet-bonding (EWB) technique has been stated to decrease degradation of resin-dentin bond. This study evaluated the effect of two EWB techniques on composite resin-to-enamel bond strength.
Silicon carbide papers were used to produce flat enamel surfaces on the buccal faces of forty-five molars. OptiBond FL (OFL) adhesive was applied on enamel surfaces in three groups of 15 namely: Enamel surface and OFL (control);Protocol 1 of the EWB technique: absolute ethanol was applied to water-saturated acid-etched enamel surfaces for 1 minute before the application of ethanol-solvated hydrophobic adhesive resin of OFL 3 times;Protocol 2: progressive ethanol replacement; water was gradually removed from the enamel matrix using ascending ethanol concentrations before OFL application. Composite build-ups were made and the specimens were stored for 24 hours at 37°C and 100% relative humidity. Shear bond strength test was performed using a universal testing machine at 1 mm/min crosshead speed. Fracture patterns were evaluated microscopically. Data were analyzed with one-way ANOVA and Fisher's exact test (α=0.05).
There were no significant differences in bond strength between the groups (P=0.73). However, regarding failure patterns, the highest cohesive enamel fractures were recorded in groups 2 and 3.
In this study, although both methods of EWB did not influence immediate bond strength of composite resin to enamel, the majority of failure patterns occurred cohesively in enamel.
乙醇湿粘结(EWB)技术据称可减少树脂-牙本质粘结的降解。本研究评估了两种EWB技术对复合树脂与牙釉质粘结强度的影响。
使用碳化硅砂纸在45颗磨牙的颊面制备平坦的牙釉质表面。在三组每组15颗的牙釉质表面上应用OptiBond FL(OFL)粘合剂,即:牙釉质表面和OFL(对照组);EWB技术方案1:在应用OFL的乙醇溶剂化疏水粘结树脂3次之前,将无水乙醇应用于水饱和酸蚀牙釉质表面1分钟;方案2:逐步乙醇置换;在应用OFL之前,使用浓度递增的乙醇逐渐从牙釉质基质中去除水分。进行复合树脂堆积,将标本在37°C和100%相对湿度下储存24小时。使用万能试验机以1 mm/min的十字头速度进行剪切粘结强度测试。通过显微镜评估断裂模式。数据采用单因素方差分析和Fisher精确检验进行分析(α=0.05)。
各组之间的粘结强度无显著差异(P=0.73)。然而,关于失败模式,在第2组和第3组中记录到最高的牙釉质内聚性骨折。
在本研究中,虽然两种EWB方法均未影响复合树脂与牙釉质的即时粘结强度,但大多数失败模式发生在牙釉质内聚性骨折。