Jayabharathi J, Karunakaran C, Kalaiarasi V, Ramanathan P, Prabhakaran A
Department of Chemistry, Annamalai University, Annamalainagar 608 002, Tamil Nadu, India.
Department of Chemistry, Annamalai University, Annamalainagar 608 002, Tamil Nadu, India.
Spectrochim Acta A Mol Biomol Spectrosc. 2015 Jan 25;135:1169-72. doi: 10.1016/j.saa.2014.07.042. Epub 2014 Jul 27.
Synthesis and characterization of 1-(naphthalene-1-yl)-2,4,5-triphenyl-1H-imidazole has been carried out by spectral studies. The synthesized phosphated imidazole and phosphated imidazole bound magnetic nanoparticles were characterized using fourier-transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS) and powder X-ray diffraction (XRD). The photophysical characteristics of the synthesized phosphated imidazole and phosphated imidazole bound magnetic nanoparticles were investigated by steady-state absorption and emission spectra as well as time resolved fluorometry. The intensities of absorption and emission maxima increase in the following order, phosphated imidazole bound Fe2O3>phosphated imidazole>imidazole.
通过光谱研究对1-(萘-1-基)-2,4,5-三苯基-1H-咪唑进行了合成与表征。使用傅里叶变换红外光谱(FT-IR)、扫描电子显微镜(SEM)、能量色散X射线光谱(EDS)和粉末X射线衍射(XRD)对合成的磷酸化咪唑和磷酸化咪唑负载磁性纳米颗粒进行了表征。通过稳态吸收和发射光谱以及时间分辨荧光法研究了合成的磷酸化咪唑和磷酸化咪唑负载磁性纳米颗粒的光物理特性。吸收和发射最大值的强度按以下顺序增加:磷酸化咪唑负载的Fe2O3>磷酸化咪唑>咪唑。