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基于X射线衍射光谱分析粉单竹微纤丝角的变化及其对拉伸性能的影响

[Variation of microfibril angle in Dendrocalamus farinosus analyzed based on X-ray diffraction spectrum and its effect on tensile properties].

作者信息

Liu Xing-e, Yang Xi, Yang Shu-min, Tian Gen-lin, Shang Li-li

出版信息

Guang Pu Xue Yu Guang Pu Fen Xi. 2014 Jun;34(6):1698-701.

Abstract

X-ray diffraction technology was used to rapidly predict variation in microfibril angle (MFA) in Dendrocalamus fari- X-ray diffraction technology was used to rapidly predict variation in microfibril angle (MFA) in Dendrocalamus farinosus. The results show that there is little variation in MFA with bamboo age from 2a to 5e, and MFA of 3a is at the maximum with the value of 8.521 degrees. The average value of MFA of 2a or 3a is greater than 4a or 5a with absolute differences less than 0.10 degrees. MFA of base, middle and upper position respectively are 8.499 degrees, 8.497 degrees and 8.483 degrees with coefficient of variation about 5%. There is an increasing tendency from the periphery to the inner of bamboo culms. Variance analysis indicates that MFA is highly sensitive to radial position, but insensitive to bamboo age and longitudinal position. The correlation coefficient of longitudinal strength and modulus of elasticity (MOE) is 0.57. MFA was responsible for 35% and 43% of the variation found in longitudinal strength and MOE respectively, which means MFA has a certain extent effect on mechanical properties.

摘要

采用X射线衍射技术快速预测粉单竹微纤丝角(MFA)的变化。结果表明,粉单竹2年生至5年生期间,微纤丝角变化不大,3年生时微纤丝角最大,为8.521度。2年生或3年生微纤丝角的平均值大于4年生或5年生,绝对差值小于0.10度。基部、中部和上部的微纤丝角分别为8.499度、8.497度和8.483度,变异系数约为5%。竹杆从外周到内部呈增加趋势。方差分析表明,微纤丝角对径向位置高度敏感,而对竹龄和纵向位置不敏感。纵向强度与弹性模量(MOE) 的相关系数为0.57。微纤丝角分别导致纵向强度和弹性模量变化的35%和43%,这意味着微纤丝角对力学性能有一定程度的影响。

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