Najafpour Mohammad Mahdi, Amini Emad
Department of Chemistry, Institute for Advanced Studies in Basic Sciences (IASBS), Zanjan, 45137-66731, Iran.
Dalton Trans. 2015 Jan 21;44(3):1039-45. doi: 10.1039/c4dt02468k.
Nanolayered Mn oxides have been prepared by a very simple, low-cost and high-yield method using soap, KOH, MnCl2 and H2O2. Scanning electron microscopy, transmission electron microscopy, dynamic light scattering, thermogravimetric analysis, Fourier transform infrared spectroscopy, and X-ray diffraction spectrometry have been used to characterize the phase and the morphology of the nanolayered Mn oxide. The nanolayered Mn oxide shows good catalytic activity toward water oxidation in the presence of cerium(iv) ammonium nitrate.
已采用一种非常简单、低成本且高产率的方法，使用肥皂、KOH、MnCl₂和H₂O₂制备了纳米层状锰氧化物。利用扫描电子显微镜、透射电子显微镜、动态光散射、热重分析、傅里叶变换红外光谱和X射线衍射光谱对纳米层状锰氧化物的相和形态进行了表征。在硝酸铈铵存在的情况下，纳米层状锰氧化物对水氧化显示出良好的催化活性。
