Elnaghy Amr M, Elsaka Shaymaa E
Faculty of Dentistry, Department of Conservative Dentistry and Endodontics, Mansoura University, Mansoura, 35516, Egypt.
Faculty of Dentistry, Department of Dental Biomaterials, Mansoura University, Mansoura, Egypt.
Odontology. 2016 Jan;104(1):60-7. doi: 10.1007/s10266-014-0184-z. Epub 2014 Nov 26.
This study evaluated the effect of different surface treatments on the flexural properties and adhesion of glass fiber post to self-adhesive luting agent and radicular dentin. Seventy-five single-rooted human teeth were prepared to receive a glass fiber post (Reblida). The posts were divided into five groups according to the surface treatment: Gr C (control; no treatment), Gr S (silanization for 60 s), Gr AP (airborne-particle abrasion), Gr HF (etching with 9 % hydrofluoric acid for 1 min), and Gr M10 (etching with CH2Cl2 for 10 min). Dual-cure self-adhesive luting agent (Rely X Unicem) was applied to each group for testing the adhesion using micropush-out test. Failure types were examined with stereomicroscope and surface morphology of the posts was characterized using a scanning electron microscopy (SEM). Flexural properties of posts were assessed using a three-point bending test. Data were analyzed using ANOVA and Tukey's HSD test. Statistical significance was set at the 0.05 probability level. Groups treated with M10 showed significantly higher bond strength than those obtained with other surface treatments (P < 0.05). In general, improvements in bond strength (MPa) were found in the following order: M10 > C > S > AP > HF. Most failure modes were adhesive type of failures between dentin and luting agent (48.2%). SEM analysis revealed that the fiber post surfaces were modified after surface treatments. The surface treatments did not compromise the flexural properties of fiber posts. Application of M10 to the fiber post surfaces enhanced the adhesion to self-adhesive luting agent and radicular dentin.
本研究评估了不同表面处理对玻璃纤维桩与自粘接树脂水门汀及牙根牙本质之间弯曲性能和粘接性能的影响。选取75颗单根人牙,预备后植入玻璃纤维桩(Reblida)。根据表面处理方法将桩分为五组:C组(对照组;未处理)、S组(硅烷化处理60秒)、AP组(空气颗粒喷砂处理)、HF组(用9%氢氟酸蚀刻1分钟)和M10组(用二氯甲烷蚀刻10分钟)。对每组均应用双固化自粘接树脂水门汀(Rely X Unicem),采用微推出试验测试粘接性能。通过体视显微镜检查失败类型,并用扫描电子显微镜(SEM)表征桩的表面形态。采用三点弯曲试验评估桩的弯曲性能。数据采用方差分析和Tukey's HSD检验进行分析。统计学显著性设定为概率水平0.05。M10组处理后的粘接强度显著高于其他表面处理组(P < 0.05)。总体而言,粘接强度(MPa)的改善顺序如下:M10 > C > S > AP > HF。大多数失败模式为牙本质与树脂水门汀之间的粘接性失败(48.2%)。SEM分析显示,表面处理后纤维桩表面发生了改变。表面处理未损害纤维桩的弯曲性能。在纤维桩表面应用M10可增强其与自粘接树脂水门汀及牙根牙本质的粘接。