Haenel Thomas, Hausnerová Berenika, Steinhaus Johannes, Price Richard B T, Sullivan Braden, Moeginger Bernhard
Centre of Polymer Systems, University Institute, Tomas Bata University in Zlin, Zlin, Czech Republic; Bonn-Rhein-Sieg, University of Applied Sciences, Department of Natural Sciences, Rheinbach, Germany.
Centre of Polymer Systems, University Institute, Tomas Bata University in Zlin, Zlin, Czech Republic; Tomas Bata University in Zlin, Faculty of Technology, Department of Production Engineering, Zlin, Czech Republic.
Dent Mater. 2015 Feb;31(2):93-104. doi: 10.1016/j.dental.2014.11.003. Epub 2014 Dec 5.
An inhomogeneous irradiance distribution from a light-curing unit (LCU) can locally cause inhomogeneous curing with locally inadequately cured and/or over-cured areas causing e.g. monomer elution or internal shrinkage stresses, and thus reduce the lifetime of dental resin based composite (RBC) restorations. The aim of the study is to determine both the irradiance distribution of two light curing units (LCUs) and its influence on the local mechanical properties of a RBC.
Specimens of Arabesk TOP OA2 were irradiated for 5, 20, and 80s using a Bluephase® 20i LCU in the Low mode (666mW/cm(2)), in the Turbo mode (2222mW/cm(2)) and a Celalux® 2 (1264mW/cm(2)). The degree of conversion (DC) was determined with an ATR-FTIR. The Knoop micro-hardness (average of five specimens) was measured on the specimen surface after 24h of dark and dry storage at room temperature.
The irradiance distribution affected the hardness distribution across the surface of the specimens. The hardness distribution corresponded well to the inhomogeneous irradiance distributions of the LCU. The highest reaction rates occurred after approximately 2s light exposure. A DC of 40% was reached after 3.6 or 5.7s, depending on the LCU. The inhomogeneous hardness distribution was still evident after 80s of light exposure.
The irradiance distribution from a LCU is reflected in the hardness distribution across the surface. Irradiance level of the LCU and light exposure time do not affect the pattern of the hardness distribution--only the hardness level. In areas of low irradiation this may result in inadequate resin polymerization, poor physical properties, and hence premature failure of the restorations as they are usually much smaller than the investigated specimens. It has to be stressed that inhomogeneous does not necessarily mean poor if in all areas of the restoration enough light intensity is introduced to achieve a high degree of cure.
光固化机(LCU)发出的不均匀辐照度分布会局部导致固化不均匀,出现局部固化不足和/或过度固化区域,从而引起例如单体洗脱或内部收缩应力,进而缩短牙科树脂基复合材料(RBC)修复体的使用寿命。本研究的目的是确定两种光固化机(LCU)的辐照度分布及其对RBC局部力学性能的影响。
使用Bluephase® 20i LCU的低模式(666mW/cm²)、Turbo模式(2222mW/cm²)以及Celalux® 2(1264mW/cm²)对Arabesk TOP OA2标本分别照射5秒、20秒和80秒。采用衰减全反射傅里叶变换红外光谱(ATR-FTIR)测定转化率(DC)。在室温下黑暗干燥储存24小时后,测量标本表面的努氏显微硬度(五个标本的平均值)。
辐照度分布影响了标本表面的硬度分布。硬度分布与LCU的不均匀辐照度分布高度吻合。光照约2秒后反应速率最高。根据所使用的LCU不同,3.6秒或5.7秒后转化率达到40%。光照80秒后,不均匀的硬度分布仍然明显。
LCU的辐照度分布反映在整个表面的硬度分布上。LCU的辐照度水平和光照时间不影响硬度分布模式——只影响硬度水平。在低辐照区域,这可能导致树脂聚合不足、物理性能不佳,从而使修复体过早失效,因为修复体通常比所研究的标本小得多。必须强调的是,如果在修复体的所有区域都引入足够的光强度以实现高度固化,不均匀并不一定意味着性能不佳。