Costa Anna Karina F, Kelly Robert D, Fleming Garry J P, Borges Alexandre Luiz S, Addison Owen
Biomaterials Unit, University of Birmingham School of Dentistry, St. Chad's Queensway, Birmingham B4 6NN, UK; Dental Materials and Prosthodontics Unit, Sao Jose dos Campos Dental School, Institute of Technology and Science, SP, Brazil.
Biomaterials Unit, University of Birmingham School of Dentistry, St. Chad's Queensway, Birmingham B4 6NN, UK.
J Dent. 2015 Mar;43(3):335-41. doi: 10.1016/j.jdent.2014.12.012. Epub 2014 Dec 30.
As CAD/CAM technologies improve we question whether adhesive lamination of ceramic materials could offer mechanical advantages over monolithic structures and improve clinical outcomes. The aim was to identify whether an adhesive interface (a chemically cured resin-cement) would influence the biaxial flexure strength (BFS) and slow-crack growth in a machinable dental ceramic.
Monolithic and adhesively laminated (with a chemically cured dimethacrylate resin-cement) feldspathic ceramic discs of identical dimensions were fabricated. BFS testing was performed on the Group A monolithic specimens (n = 20), on Group B laminated specimens with the adhesive interface positioned below the neutral bending axis (n = 20) and Group C laminated specimens with the adhesive interface positioned above the neutral bending axis (n = 20). To study subcritical crack growth additional laminated specimens received controlled indentations and were exposed to thermo-mechanical fatigue. BFS data was analysed using parametric statistics (α = 0.05). Fractographic analyses were qualitatively assessed.
No significant differences between the mean BFS data of Groups A and B were observed (p = 0.92) but the mean BFS of Group C was slightly reduced (p < 0.01). Lamination reduced the stiffness of the structure and fractographic analysis demonstrated that energy consuming crack deflection occurred. Thermo-mechanical fatigue caused subcritical extension of radial cracks associated with indentations adjacent to the adhesive interface. Crack growth was limited to parallel to the interface and was arrested or deflected in a direction normal to the interface.
Ceramic lamination increased the damage tolerance of the structure and could limit or arrest subcritical crack growth at regions near the 'interlayer'.
Lamination of a dental ceramic with a polymeric 'interlayer' could offer toughening effects which could potentially delay or arrest sub-critical crack growth at regions near the interface and thereby improve restoration longevity.
随着计算机辅助设计/计算机辅助制造(CAD/CAM)技术的进步,我们探讨陶瓷材料的粘结层压是否能比整体结构提供机械优势并改善临床效果。目的是确定粘结界面(化学固化树脂水门汀)是否会影响可加工牙科陶瓷的双轴弯曲强度(BFS)和慢裂纹扩展。
制作尺寸相同的整体式和粘结层压(使用化学固化的二甲基丙烯酸酯树脂水门汀)长石质陶瓷圆盘。对A组整体试样(n = 20)、B组粘结界面位于中性弯曲轴下方的层压试样(n = 20)和C组粘结界面位于中性弯曲轴上方的层压试样(n = 20)进行BFS测试。为研究亚临界裂纹扩展,额外的层压试样接受受控压痕并进行热机械疲劳试验。使用参数统计分析BFS数据(α = 0.05)。对断口分析进行定性评估。
未观察到A组和B组平均BFS数据之间存在显著差异(p = 0.92),但C组的平均BFS略有降低(p < 0.01)。层压降低了结构的刚度,断口分析表明发生了耗能裂纹偏转。热机械疲劳导致与粘结界面相邻压痕相关的径向裂纹亚临界扩展。裂纹扩展仅限于平行于界面,并在垂直于界面的方向上停止或偏转。
陶瓷层压提高了结构的损伤容限,并可在“中间层”附近区域限制或阻止亚临界裂纹扩展。
用聚合物“中间层”对牙科陶瓷进行层压可提供增韧效果,这可能会延迟或阻止界面附近区域的亚临界裂纹扩展,从而提高修复体的使用寿命。