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有机非线性光学材料:丙酸氯倍他索的生长与表征

Growth and characterization of organic NLO material: clobetasol propionate.

作者信息

Purusothaman R, Rajesh P, Ramasamy P

机构信息

Department of Physics, SSN college of Engineering, Kalavakkam 603 110, India.

Department of Physics, SSN college of Engineering, Kalavakkam 603 110, India.

出版信息

Spectrochim Acta A Mol Biomol Spectrosc. 2015 Jun 15;145:235-238. doi: 10.1016/j.saa.2015.03.014. Epub 2015 Mar 10.

DOI:10.1016/j.saa.2015.03.014
PMID:25791879
Abstract

Single crystals of clobetasol propionate (CP) have been grown by slow evaporation solution technique using mixed solvent of methanol-acetone. The grown crystals were subjected to single crystal X-ray diffraction analysis to confirm their lattice parameter and space group. The powder X-ray diffraction pattern of the grown CP has been indexed. Thermal analysis was performed to study the thermal stability of the grown crystals. Photoluminescence spectrum shows broad emission peak observed at 421 nm. Nonlinear optical studies were carried out for the grown crystal and second harmonic generation (SHG) efficiency was found in the crystal.

摘要

已通过使用甲醇 - 丙酮混合溶剂的缓慢蒸发溶液技术生长出丙酸氯倍他索(CP)的单晶。对生长出的晶体进行了单晶X射线衍射分析,以确认其晶格参数和空间群。已对生长出的CP的粉末X射线衍射图谱进行了索引。进行了热分析以研究生长出的晶体的热稳定性。光致发光光谱显示在421nm处观察到宽发射峰。对生长出的晶体进行了非线性光学研究,并且在该晶体中发现了二次谐波产生(SHG)效率。

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