Bilge Gonca, Boyacı İsmail Hakkı, Eseller Kemal Efe, Tamer Uğur, Çakır Serhat
Department of Food Engineering, Hacettepe University, Beytepe, 06800 Ankara, Turkey.
Department of Food Engineering, Hacettepe University, Beytepe, 06800 Ankara, Turkey; Food Research Center, Hacettepe University, Beytepe, 06800 Ankara, Turkey.
Food Chem. 2015 Aug 15;181:186-90. doi: 10.1016/j.foodchem.2015.02.090. Epub 2015 Feb 24.
In this study, we focused on the detection of Na in bakery products by using laser-induced breakdown spectroscopy (LIBS) as a quick and simple method. LIBS experiments were performed to examine the Na at 589 nm to quantify NaCl. A series of standard bread sample pellets containing various concentrations of NaCl (0.025-3.5%) were used to construct the calibration curves and to determine the detection limits of the measurements. Calibration graphs were drawn to indicate functions of NaCl and Na concentrations, which showed good linearity in the range of 0.025-3.5% NaCl and 0.01-1.4% Na concentrations with correlation coefficients (R(2)) values greater than 0.98 and 0.96. The obtained detection limits for NaCl and Na were 175 and 69 ppm, respectively. Performed experimental studies showed that LIBS is a convenient method for commercial bakery products to quantify NaCl concentrations as a rapid and in situ technique.
在本研究中,我们重点使用激光诱导击穿光谱法(LIBS)作为一种快速简便的方法来检测烘焙食品中的钠。进行LIBS实验以检测589nm处的钠,从而对氯化钠进行定量。使用一系列含有不同浓度氯化钠(0.025 - 3.5%)的标准面包样品颗粒来构建校准曲线并确定测量的检测限。绘制校准图以显示氯化钠和钠浓度的函数关系,其在0.025 - 3.5%氯化钠和0.01 - 1.4%钠浓度范围内显示出良好的线性,相关系数(R²)值大于0.98和0.96。所获得的氯化钠和钠的检测限分别为175ppm和69ppm。进行的实验研究表明,LIBS作为一种快速且原位的技术,是用于商业烘焙食品中氯化钠浓度定量的便捷方法。