亚硫酸钠、羧酸单体和磷酸蚀刻对三正丁基硼烷引发树脂与人类牙釉质粘结的影响。

Effect of sodium sulfite, carboxylic monomer, and phosphoric acid etching on bonding of tri-n-butylborane initiated resin to human enamel.

作者信息

Nogawa Hiroshi, Koizumi Hiroyasu, Akazawa Nobutaka, Hiraba Haruto, Nakamura Mitsuo, Matsumura Hideo

机构信息

Division of Applied Oral Science, Nihon University Graduate School of Dentistry.

出版信息

J Oral Sci. 2015 Mar;57(1):17-24. doi: 10.2334/josnusd.57.17.

DOI:10.2334/josnusd.57.17

PMID:25807904

Abstract

The purpose of the present study is evaluation of bonding durability of tri-n-butylborane (TBB) initiated resin without 4-methacryloyloxyethyl trimellitate anhydride (4-META) joined to human enamel. Ground human enamel was bonded with TBB resin under six surface conditions: 1) as ground, 2) primed with Teeth Primer, 3) sodium sulfite solution, 4) 4-META solution, 5) acetone-water, and 6) phosphoric acid etching. Pre- and post-thermocycling bond strengths and change in strength after thermocycling were compared. Etching enamel with 35-45% phosphoric acid enhanced bonding durability between enamel and TBB-initiated resin. Priming with Teeth Primer or 4-META solution improved bond strength between enamel and TBB-initiated resin. Sodium sulfite had little effect on enamel bonding in the present bonding systems.

摘要

本研究的目的是评估不含4-甲基丙烯酰氧基乙基偏苯三酸酐（4-META）的三正丁基硼烷（TBB）引发树脂与人类牙釉质的粘结耐久性。将磨碎的人类牙釉质在六种表面条件下与TBB树脂粘结：1）磨碎后；2）用牙齿底漆预处理；3）亚硫酸钠溶液处理；4）4-META溶液处理；5）丙酮-水处理；6）磷酸蚀刻处理。比较了热循环前后的粘结强度以及热循环后的强度变化。用35%-45%的磷酸蚀刻牙釉质可提高牙釉质与TBB引发树脂之间的粘结耐久性。用牙齿底漆或4-META溶液预处理可提高牙釉质与TBB引发树脂之间的粘结强度。在本粘结体系中，亚硫酸钠对牙釉质粘结几乎没有影响。