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2
The application of solid-phase micro-extraction (SPME) to the analysis of polycyclic aromatic hydrocarbons (PAHs).
Environ Geochem Health. 2003 Mar;25(1):69-75. doi: 10.1023/a:1021248932084.
3
Use of gas chromatography-olfactometry to identify key odorant compounds in dark chocolate. Comparison of samples before and after conching.使用气相色谱 - 嗅觉测量法鉴定黑巧克力中的关键气味化合物。精磨前后样品的比较。
J Agric Food Chem. 2002 Apr 10;50(8):2385-91. doi: 10.1021/jf0114177.
4
Analysis of low-volatility organic sulphur compounds in wines by solid-phase microextraction and gas chromatography.采用固相微萃取和气相色谱法分析葡萄酒中的低挥发性有机硫化合物
J Chromatogr A. 2000 Jun 9;881(1-2):583-90. doi: 10.1016/s0021-9673(00)00326-5.

精磨过程中添加肉桂粉对黑巧克力酱风味的影响。

Effect of cinnamon powder addition during conching on the flavor of dark chocolate mass.

作者信息

Albak F, Tekin A R

机构信息

Department of Engineering, Gaziantep University, 27310 Gaziantep, Turkey.

出版信息

J Food Sci Technol. 2015 Apr;52(4):1960-70. doi: 10.1007/s13197-013-1217-2. Epub 2013 Nov 30.

DOI:10.1007/s13197-013-1217-2
PMID:25829576
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC4375175/
Abstract

In the present study, refined dark chocolate mix was conched with the addition of finely powdered cinnamon in a laboratory-style conching machine to evaluate its aroma profile both analytically and sensorially. The analytical determinations were carried out by a combination of solid phase micro extraction (SPME)-gas chromatography (GC)-mass spectroscopy (MS) and-olfactometry(O), while the sensory evaluation was made with trained panelists. The optimum conditions for the SPME were found to be CAR/PDMS as the fiber, 60 °C as the temperature, and 60 min as the time. SPME analyses were carried out at 60 °C for 60 min with toluene as an internal standard. 26 compounds were monitored before and after conching. The unconched sample had a significantly higher fruity odor value than the conched sample. This new product was highly acceptable according to the overall inclination test. However some of textural properties, such as coarseness, and hardness were below the general preference.

摘要

在本研究中,将精制黑巧克力混合物与细粉状肉桂一起在实验室风格的精磨机中进行精磨,以从分析和感官两方面评估其香气特征。分析测定通过固相微萃取(SPME)-气相色谱(GC)-质谱(MS)联用嗅觉测定法(O)进行,而感官评价则由经过培训的评审员完成。发现SPME的最佳条件为使用CAR/PDMS作为纤维、60°C作为温度、60分钟作为时间。以甲苯为内标,在60°C下进行60分钟的SPME分析。在精磨前后监测了26种化合物。未精磨的样品比精磨后的样品具有显著更高的果香气味值。根据总体倾向测试,该新产品非常受欢迎。然而,一些质地特性,如粗糙度和硬度低于一般偏好。