4-甲基-N-[(4-甲基吡啶-2-基)氨基甲酰硫基]-苯甲酰胺的晶体结构
Crystal structure of 4-methyl-N-[(4-methyl-pyridin-2-yl)carbamo-thioyl]-benzamide.
作者信息
Adam Farook, Ameram Nadiah, Eltayeb Naser Eltaher
机构信息
School of Chemical Sciences, 11800, USM Pulau Pinang, Malaysia.
College of Sciences and Arts, Rabigh, King Abdulaziz University, Saudi Arabia, and International University of Africa, Khartoum, Sudan.
出版信息
Acta Crystallogr E Crystallogr Commun. 2015 Feb 28;71(Pt 3):315-7. doi: 10.1107/S2056989015003412. eCollection 2015 Mar 1.
In the title compound, C15H15N3OS, the dihedral angle between the planes of the benzene and pyridine rings is 26.86 (9)°. Intra-molecular N-H⋯O and C-H⋯S hydrogen bonds both generate S(6) rings. The C=O and C=S bonds lie to opposite sides of the mol-ecule. In the crystal, inversion dimers linked by pairs of N-H⋯S hydrogen bonds generate R 2 (2)(8) loops.
在标题化合物C₁₅H₁₅N₃OS中，苯环和吡啶环平面之间的二面角为26.86 (9)°。分子内的N-H⋯O和C-H⋯S氢键均形成S(6)环。C=O键和C=S键位于分子的相反两侧。在晶体中，通过成对的N-H⋯S氢键相连的反演二聚体形成R 2 (2)(8)环。
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