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用于砂岩三维及准三维化学和结构表征的高分辨率X射线CT、扫描电子显微镜和能谱仪的数据融合

Data-fusion of high resolution X-ray CT, SEM and EDS for 3D and pseudo-3D chemical and structural characterization of sandstone.

作者信息

De Boever Wesley, Derluyn Hannelore, Van Loo Denis, Van Hoorebeke Luc, Cnudde Veerle

机构信息

PProGRess-UGCT, Department of Geology and Soil Science, Ghent University, Ghent, Belgium.

PProGRess-UGCT, Department of Geology and Soil Science, Ghent University, Ghent, Belgium.

出版信息

Micron. 2015 Jul;74:15-21. doi: 10.1016/j.micron.2015.04.003. Epub 2015 Apr 17.

Abstract

When dealing with the characterization of the structure and composition of natural stones, problems of representativeness and choice of analysis technique almost always occur. Since feature-sizes are typically spread over the nanometer to centimeter range, there is never one single technique that allows a rapid and complete characterization. Over the last few decades, high resolution X-ray CT (μ-CT) has become an invaluable tool for the 3D characterization of many materials, including natural stones. This technique has many important advantages, but there are also some limitations, including a tradeoff between resolution and sample size and a lack of chemical information. For geologists, this chemical information is of importance for the determination of minerals inside samples. We suggest a workflow for the complete chemical and structural characterization of a representative volume of a heterogeneous geological material. This workflow consists of combining information derived from CT scans at different spatial resolutions with information from scanning electron microscopy and energy-dispersive X-ray spectroscopy.

摘要

在处理天然石材的结构和组成特征时,代表性问题和分析技术的选择问题几乎总是会出现。由于特征尺寸通常分布在纳米到厘米范围内,从来没有一种单一的技术能够实现快速且完整的表征。在过去几十年中,高分辨率X射线计算机断层扫描(μ-CT)已成为对包括天然石材在内的许多材料进行三维表征的宝贵工具。该技术具有许多重要优点,但也存在一些局限性,包括分辨率与样品尺寸之间的权衡以及缺乏化学信息。对于地质学家而言,这种化学信息对于确定样品内部的矿物至关重要。我们提出了一种用于对非均质地质材料的代表性体积进行完整化学和结构表征的工作流程。该工作流程包括将来自不同空间分辨率的CT扫描获得的信息与扫描电子显微镜和能量色散X射线光谱学的信息相结合。

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