Rirattanapong P, Senawongse P, Harnirattisal C, Wunsiw W
J Clin Pediatr Dent. 2015 Spring;39(3):224-30. doi: 10.17796/1053-4628-39.3.224.
The aim of this study was to evaluate the effects of a smear layer generated by a high-speed diamond or carbide bur on the durability of microtensile bond strength (μTBS) of a self-etching adhesive to primary dentin.
Flat occlusal dentin surfaces of 105 human primary molars were exposed using 600 grit silicon carbide paper before being divided into 2 groups for further grinding with either a highspeed diamond or carbide bur. Ten prepared dentin surfaces treated by each bur were evaluated for the characteristics of the smear layer using a scanning electron microscope (SEM). Seventy-five specimens from each bur-prepared group were applied with a 2-step self-etching adhesive (Clearfil SE Bond(®)) then built up with a resin composite. Each bonded specimen was sectioned into a 1-mm thick slab and trimmed to a dumbbell shape with a cross-sectional area of approximately 1 mm(2). All slabs were divided into 3 groups (n=25) according to 3 storage times of 24 hrs, 3 months, and 6 months, in distilled water at 37°C. After storage, the μTBS was determined using a universal testing machine. All fracture specimens were prepared for observation of failure modes. Ten bonded specimens of each bur group were prepared for observation of the resin-dentin interface using an SEM. Smear-layer thickness, μTBS, and failure mode distributions were statistically analyzed.
The high speed carbide bur created a significantly thinner smear layer than the diamond bur (p < 0.05). Dentin surfaces treated with a high-speed carbide bur generally obtained significantly higher μTBS than the diamond bur group (p < 0.05). The μTBS gradually decreased over time such that specimens stored for 6 months had significantly lower bond strength than those stored for 24 hrs (p < 0.05). Self-etching adhesive created a hybrid layer of the same thickness when prepared with either a carbide bur or diamond bur, but the carbide bur group had longer and more resin tags.
Highspeed carbide bur groups had a higher μTBS than diamond bur groups for all storage times, and bond strengths decreased over time in both substrate groups. The use of a carbide bur produced a thinner smear layer and therefore is recommended when using this 2-step self-etching adhesive to bond the resin composite to primary dentin.
本研究旨在评估高速金刚石或硬质合金车针产生的玷污层对自酸蚀黏结剂与乳牙本质微拉伸黏结强度(μTBS)耐久性的影响。
用600目碳化硅砂纸打磨105颗人乳牙的平坦咬合面牙本质表面,然后将其分为2组,分别用高速金刚石或硬质合金车针进一步打磨。使用扫描电子显微镜(SEM)评估每种车针处理的10个制备好的牙本质表面玷污层的特征。每组用每种车针制备的75个标本应用两步自酸蚀黏结剂(Clearfil SE Bond(®)),然后用树脂复合材料堆积。将每个黏结标本切成1毫米厚的薄片,修剪成横截面面积约为1平方毫米的哑铃形。所有薄片根据在37℃蒸馏水中24小时、3个月和6个月的3个储存时间分为3组(n = 25)。储存后,使用万能试验机测定μTBS。制备所有断裂标本以观察失败模式。每组每种车针制备的10个黏结标本用SEM观察树脂-牙本质界面。对玷污层厚度、μTBS和失败模式分布进行统计分析。
高速硬质合金车针产生的玷污层明显比金刚石车针薄(p < 0.05)。用高速硬质合金车针处理的牙本质表面通常比金刚石车针组获得明显更高的μTBS(p < 0.05)。μTBS随时间逐渐降低,以至于储存6个月的标本的黏结强度明显低于储存24小时的标本(p < 0.05)。用硬质合金车针或金刚石车针制备时,自酸蚀黏结剂产生的混合层厚度相同,但硬质合金车针组的树脂突更长且更多。
在所有储存时间内,高速硬质合金车针组的μTBS均高于金刚石车针组,且两个基底组的黏结强度均随时间下降。使用硬质合金车针产生的玷污层更薄,因此在使用这种两步自酸蚀黏结剂将树脂复合材料黏结到乳牙本质时推荐使用。