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采用微波蒸馏-顶空单滴微萃取-气相色谱-质谱联用（GC-MS）法快速分析细叶蓍的挥发性成分。

Fast analysis of volatile components of Achillea tenuifolia Lam with microwave distillation followed by headspace single-drop microextraction coupled to gas chromatography-mass spectrometry (GC-MS).

作者信息

Piryaei Marzieh, Nazemiyeh Hossein

机构信息

a Research Center for Pharmaceutical Nanotechnology , Tabriz University of Medical Sciences , Tabriz , Iran.

b Faculty of Pharmacy , Tabriz University of Medical Sciences , Tabriz , Iran.

出版信息

Nat Prod Res. 2016;30(8):991-4. doi: 10.1080/14786419.2015.1079911. Epub 2015 Sep 2.

DOI:10.1080/14786419.2015.1079911
PMID:26329700
Abstract

This article investigates the effect of microwaves on the amount of volatile compounds Achillea tenuifolia Lam with two methods, headspace single-drop microextraction and microwave-assisted headspace single-drop microextraction (MA-SDME), for the analysis of essential oil. Solvent selection, solvent volume, microwave power, irradiation time and sample mass were optimised by the simplex method.

摘要

本文采用顶空单滴微萃取和微波辅助顶空单滴微萃取（MA-SDME）两种方法研究微波对细叶蓍挥发性化合物含量的影响，以分析其精油。采用单纯形法对溶剂选择、溶剂量、微波功率、辐照时间和样品质量进行了优化。

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