Ren Jiabao, Lin Hong, Huang Qingmei, Liang Qifan, Zheng Gang
Department of Dental Materials, School of Stomatology, Peking University, Beijing, China.
National Engineering Laboratory for Digital and Material Technology of Stomatology, Peking University, Beijing, China.
Biomed Mater Eng. 2015;26 Suppl 1:S35-43. doi: 10.3233/BME-151287.
This study aimed to set evaluation indicators, i.e., perceptibility and acceptability color difference thresholds, of color stability for acrylic denture base resins for a spectrophotometric assessing method, which offered an alternative to the visual method described in ISO 20795-1:2013. A total of 291 disk specimens 50±1 mm in diameter and 0.5±0.1 mm thick were prepared (ISO 20795-1:2013) and processed through radiation tests in an accelerated aging chamber (ISO 7491:2000) for increasing times of 0 to 42 hours. Color alterations were measured with a spectrophotometer and evaluated using the CIE Lab* colorimetric system. Color differences were calculated through the CIEDE2000 color difference formula. Thirty-two dental professionals without color vision deficiencies completed perceptibility and acceptability assessments under controlled conditions in vitro. An S-curve fitting procedure was used to analyze the 50:50% perceptibility and acceptability thresholds. Furthermore, perceptibility and acceptability against the differences of the three color attributes, lightness, chroma, and hue, were also investigated. According to the S-curve fitting procedure, the 50:50% perceptibility threshold was 1.71ΔE00 (r(2)=0.88) and the 50:50% acceptability threshold was 4.00 ΔE00 (r(2)=0.89). Within the limitations of this study, 1.71/4.00 ΔE00 could be used as perceptibility/acceptability thresholds for acrylic denture base resins.
本研究旨在为分光光度评估法设定丙烯酸义齿基托树脂颜色稳定性的评估指标,即可察觉性和可接受性色差阈值,该方法为ISO 20795-1:2013中所述的视觉方法提供了一种替代方案。共制备了291个直径50±1mm、厚度0.5±0.1mm的圆盘试样(ISO 20795-1:2013),并在加速老化箱中进行辐射试验(ISO 7491:2000),时间从0小时增加到42小时。用分光光度计测量颜色变化,并使用CIE Lab*比色系统进行评估。通过CIEDE2000色差公式计算色差。32名无色觉缺陷的牙科专业人员在体外受控条件下完成了可察觉性和可接受性评估。采用S曲线拟合程序分析50:50%的可察觉性和可接受性阈值。此外,还研究了针对明度、彩度和色调这三种颜色属性差异的可察觉性和可接受性。根据S曲线拟合程序,50:50%的可察觉性阈值为1.71ΔE00(r(2)=0.88),50:50%的可接受性阈值为4.00ΔE00(r(2)=0.89)。在本研究的局限性内,1.71/4.00ΔE00可作为丙烯酸义齿基托树脂的可察觉性/可接受性阈值。