• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利:CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验

通过洪斯迪克尔反应制备氟官能化氧化石墨烯

Preparation of fluoro-functionalized graphene oxide via the Hunsdiecker reaction.

作者信息

Xing Ruiguang, Li Yanan, Yu Huitao

机构信息

School of Materials and Metallurgy, Inner Mongolia University of Science and Technology, No. 7 Arding Street, Kun District, Baotou 014010, China.

出版信息

Chem Commun (Camb). 2016 Jan 7;52(2):390-3. doi: 10.1039/c5cc08252h. Epub 2015 Nov 2.

DOI:10.1039/c5cc08252h
PMID:26524464
Abstract

We report our effort in the development of a new synthetic method for fluoro-functionalized graphene oxide, which was prepared via the Hunsdiecker reaction, and the treatment of carboxylated graphene oxide with selectfluor at 90°C for 10 h under an atmosphere of nitrogen, using silver nitrate as a catalyst.

摘要

我们报告了我们在开发一种用于氟官能化氧化石墨烯的新合成方法方面所做的努力,该方法是通过洪斯迪克尔反应制备的,即在氮气气氛下,使用硝酸银作为催化剂,在90°C下用Selectfluor处理羧基化氧化石墨烯10小时。

相似文献

1
Preparation of fluoro-functionalized graphene oxide via the Hunsdiecker reaction.通过洪斯迪克尔反应制备氟官能化氧化石墨烯
Chem Commun (Camb). 2016 Jan 7;52(2):390-3. doi: 10.1039/c5cc08252h. Epub 2015 Nov 2.
2
Selective Bromination of Graphene Oxide by the Hunsdiecker Reaction.通过洪斯迪克尔反应对氧化石墨烯进行选择性溴化
Chemistry. 2017 Aug 1;23(43):10473-10479. doi: 10.1002/chem.201702031. Epub 2017 Jul 11.
3
Graphene oxide functionalized with silver@silica-polyethylene glycol hybrid nanoparticles for direct electrochemical detection of quercetin.银@二氧化硅-聚乙二醇杂化纳米粒子功能化的氧化石墨烯用于槲皮素的直接电化学检测。
Biosens Bioelectron. 2014 Aug 15;58:200-4. doi: 10.1016/j.bios.2014.02.062. Epub 2014 Mar 5.
4
Selective nitrogen functionalization of graphene by Bucherer-type reaction.通过布赫尔型反应对石墨烯进行选择性氮官能化。
Chemistry. 2015 May 26;21(22):8090-5. doi: 10.1002/chem.201405748. Epub 2015 Mar 26.
5
Continuous production of nitrogen-functionalized graphene nanosheets for catalysis applications.用于催化应用的氮功能化石墨烯纳米片的连续生产。
Nanoscale. 2014 Nov 7;6(21):12758-68. doi: 10.1039/c4nr02824d.
6
Preparation and characterization of a composite hydrogel with graphene oxide as an acid catalyst.以氧化石墨烯为酸催化剂的复合水凝胶的制备与表征
Soft Matter. 2015 Apr 28;11(16):3215-21. doi: 10.1039/c5sm00142k.
7
Preparation of nitrogen-doped graphene sheets by a combined chemical and hydrothermal reduction of graphene oxide.通过氧化石墨烯的化学和水热还原联合制备氮掺杂石墨烯片。
Langmuir. 2010 Oct 19;26(20):16096-102. doi: 10.1021/la102425a.
8
Nitrogen-Doped Reduced Graphene Oxide Prepared by Simultaneous Thermal Reduction and Nitrogen Doping of Graphene Oxide in Air and Its Application as an Electrocatalyst.氮气掺杂还原氧化石墨烯的制备及其在空气中同时热还原和氮掺杂氧化石墨烯作为电催化剂的应用。
ACS Appl Mater Interfaces. 2015 Dec 9;7(48):26952-8. doi: 10.1021/acsami.5b07757. Epub 2015 Nov 25.
9
Porous nitrogen-doped carbon nanosheet on graphene as metal-free catalyst for oxygen reduction reaction in air-cathode microbial fuel cells.在空气阴极微生物燃料电池中,作为无金属催化剂的多孔氮掺杂碳纳米片在石墨烯上用于氧还原反应。
Bioelectrochemistry. 2014 Feb;95:23-8. doi: 10.1016/j.bioelechem.2013.10.007. Epub 2013 Oct 25.
10
Highly efficient and recyclable nanocomplexed photocatalysts of AgBr/N-doped and amine-functionalized reduced graphene oxide.具有高效和可回收性的 AgBr/N 掺杂和胺功能化还原氧化石墨烯纳米复合物光催化剂。
ACS Appl Mater Interfaces. 2014 Dec 10;6(23):20819-27. doi: 10.1021/am5051422. Epub 2014 Nov 25.

引用本文的文献

1
The effects of formation and functionalization of graphene-based membranes on their gas and water vapor permeation properties.基于石墨烯的膜的形成和功能化对其气体和水蒸气渗透性能的影响。
Heliyon. 2023 Oct 21;9(11):e21417. doi: 10.1016/j.heliyon.2023.e21417. eCollection 2023 Nov.
2
l-Ascorbic Acid Treatment of Electrochemical Graphene Nanosheets: Reduction Optimization and Application for De-Icing, Water Uptake Prevention, and Corrosion Resistance.l-抗坏血酸处理电化学石墨烯纳米片:还原优化及其在除冰、防吸水和耐腐蚀性方面的应用。
ACS Appl Mater Interfaces. 2023 May 10;15(18):22471-22484. doi: 10.1021/acsami.2c22854. Epub 2023 Apr 26.
3
Development and Up-Scaling of Electrochemical Production and Mild Thermal Reduction of Graphene Oxide.
氧化石墨烯的电化学生产及温和热还原的发展与放大
Materials (Basel). 2022 Jul 1;15(13):4639. doi: 10.3390/ma15134639.
4
Synthesis of 1,3-dicarbonyl-functionalized reduced graphene oxide/MnO composites and their electrochemical properties as supercapacitors.1,3-二羰基官能化还原氧化石墨烯/MnO复合材料的合成及其作为超级电容器的电化学性能
RSC Adv. 2018 Mar 21;8(21):11338-11343. doi: 10.1039/c7ra13394d.
5
Decarboxylative Halogenation of Organic Compounds.有机化合物的脱羧卤化反应。
Chem Rev. 2021 Jan 13;121(1):412-484. doi: 10.1021/acs.chemrev.0c00813. Epub 2020 Nov 17.
6
Piezoelectric Response in Electrospun Poly(vinylidene fluoride) Fibers Containing Fluoro-Doped Graphene Derivatives.含氟掺杂石墨烯衍生物的电纺聚偏氟乙烯纤维中的压电响应
ACS Omega. 2018 May 17;3(5):5317-5326. doi: 10.1021/acsomega.8b00237. eCollection 2018 May 31.
7
High-efficient Synthesis of Graphene Oxide Based on Improved Hummers Method.基于改进的Hummers法高效合成氧化石墨烯
Sci Rep. 2016 Nov 3;6:36143. doi: 10.1038/srep36143.