Wang Chen-guang, Yang Jiang-tao, Kang Ning, Guo Hao, Tang Jun, Liu Jun, Xue Chen-yang
Guang Pu Xue Yu Guang Pu Fen Xi. 2015 Dec;35(12):3529-33.
Because traditional method for tunable grating fabrication has harsh process condition, complex fabrication process, high costs and long cycle. Proposed a low-cost, simple process, can be prepared in large quantities gradient grating process method, based on self-assembly process using the rigid film/flexible substrate and oxygen plasma method prepared a micron scale gradient grating. Use of plasma free time controllability and excellent elastic of PDMS obtained the desired grating. First, polyethylene terephthalate (PET) was spin-coated layer of polydimethylsiloxane (PDMS) film on the thin film, two-layer film to be cured PDMS film after bending and treated with an oxygen plasma (plasma), in generating a rigid surface oxide layer, With flexible PET rigid layer applied uniform stress, when the stress exceeds the critical value, the PDMS substrate to form a self-assembled structure grating fold. Due to changes in prestressed bending, so the PDMS film formation period and height of the grating stepped fold, which is graded grating. Using visible light as the performance test light source for graded grating and selecting first-order diffracted as the detection target. The authors can see the grating has a good diffraction effects and achieves good spectral effect. Experiments show that graded grating has obvious diffraction grating, and the diffraction angle varies significantly, and can be widely used for stress measurement, the flexible gradient grating prepared by this method can also be used to detect changes in the stress strain as a miniature device, the future is expected for miniature spectrometer, scanners, optical communications and other fields.
由于传统的可调谐光栅制造方法工艺条件苛刻、制造过程复杂、成本高且周期长。提出了一种低成本、工艺简单、可大量制备的梯度光栅工艺方法,基于自组装工艺,利用刚性薄膜/柔性衬底并采用氧等离子体法制备了微米级梯度光栅。利用等离子体自由时间的可控性和聚二甲基硅氧烷(PDMS)优异的弹性获得了所需的光栅。首先,在聚对苯二甲酸乙二醇酯(PET)薄膜上旋涂一层聚二甲基硅氧烷(PDMS)薄膜,两层薄膜弯曲后对PDMS薄膜进行固化并经氧等离子体(等离子体)处理,在表面生成刚性氧化层,对柔性PET刚性层施加均匀应力,当应力超过临界值时,PDMS衬底形成自组装结构的褶皱光栅。由于预应力弯曲的变化,所以PDMS薄膜形成的光栅褶皱周期和高度呈阶梯状,即梯度光栅。以可见光作为梯度光栅的性能测试光源并选取一级衍射光作为检测目标。作者可以看到光栅具有良好的衍射效果并实现了良好的光谱效应。实验表明梯度光栅具有明显的光栅衍射,且衍射角变化显著,可广泛用于应力测量,通过该方法制备的柔性梯度光栅还可作为微型器件用于检测应力应变的变化,未来有望应用于微型光谱仪、扫描仪、光通信等领域。