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参与COST行动-TU1301“建筑中的天然放射性核素(NORM4Building)”的各实验室间的首次比对:陶瓷中天然放射性核素的测定

First intercomparison among laboratories involved in COST Action-TU1301 "NORM4Building": Determination of natural radionuclides in ceramics.

作者信息

Xhixha Gerti, Trinidad José Antonio, Gascó Catalina, Mantovani Fabio

机构信息

Legnaro National Laboratory - National Institute of Nuclear Physics (INFN), Via dell'Università, 2 - 35020 Legnaro, Padova, Italy; Department of Physics, Faculty of Natural Sciences, University of Tirana, Blv. Zogu I, 1001 Tirana, Albania.

Unit of Environmental Radioactivity and Radiological Surveillance, CIEMAT, Avda de la Complutense, 40 - 28040 Madrid, Spain.

出版信息

J Environ Radioact. 2017 Mar;168:4-9. doi: 10.1016/j.jenvrad.2016.03.007. Epub 2016 Mar 19.

Abstract

This work describes the outcomes of the COST Action-TU1301 "NORM4Building" intercomparison on the determination of natural radioactivity in ceramics. Twenty-two laboratories involved in the intercomparison are evaluated for their performance using robust statistics. The reference values of Ra (Bi and Pb) are determined to be 122 ± 11 Bq kg and 124 ± 14 Bq kg, respectively and in secular equilibrium in the uranium chain while the reference values of Th (Ac) is determined to be 61 ± 6 Bq kg and that of K was determined to be 955 ± 40 Bq kg. Although the aim of the exercise was to determine the activity concentration of Ra, Th and K and evaluation of the "Activity Concentration Index", laboratories were asked to report complete characterization of natural radionuclides. The results of this exercise pointed out a good performance among laboratories since the percentage of the acceptable results were above 90% for the radionuclides of interest. Based on these results, considering the systematic rejection of the results reported from a few laboratories we emphasize the need for quality control procedures.

摘要

这项工作描述了COST行动-TU1301“NORM4Building”关于陶瓷中天然放射性测定的比对结果。对参与比对的22个实验室的性能进行了稳健统计评估。镭(铋和铅)的参考值分别确定为122±11 Bq/kg和124±14 Bq/kg,在铀系中处于长期平衡状态,钍(锕)的参考值确定为61±6 Bq/kg,钾的参考值确定为955±40 Bq/kg。尽管此次活动的目的是确定镭、钍和钾的活度浓度以及评估“活度浓度指数”,但要求实验室报告天然放射性核素的完整特征。此次活动的结果表明实验室之间表现良好,因为感兴趣的放射性核素的可接受结果百分比高于90%。基于这些结果,考虑到少数实验室报告结果被系统剔除的情况,我们强调了质量控制程序的必要性。

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