Holm Jason, Keller Robert R
National Institute of Standards and Technology, Applied Chemicals and Materials Division, 325 Broadway, Boulder, CO 80305, United States.
National Institute of Standards and Technology, Applied Chemicals and Materials Division, 325 Broadway, Boulder, CO 80305, United States.
Ultramicroscopy. 2016 Aug;167:43-56. doi: 10.1016/j.ultramic.2016.05.001. Epub 2016 May 5.
This work presents recent advances in transmission scanning electron microscopy (t-SEM) imaging control capabilities. A modular aperture system and a cantilever-style sample holder that enable comprehensive angular selectivity of forward-scattered electrons are described. When combined with a commercially available solid-state transmission detector having only basic bright-field and dark-field imaging capabilities, the advances described here enable numerous transmission imaging modes. Several examples are provided that demonstrate how contrast arising from diffraction to mass-thickness can be obtained. Unanticipated image contrast at some imaging conditions is also observed and addressed.
这项工作展示了透射扫描电子显微镜(t-SEM)成像控制能力的最新进展。描述了一种模块化孔径系统和一种悬臂式样品架,它们能够实现前向散射电子的全面角度选择性。当与仅具有基本明场和暗场成像能力的市售固态透射探测器结合使用时,本文所述的进展实现了多种透射成像模式。提供了几个示例,展示了如何获得从衍射到质量厚度产生的对比度。还观察并解决了在某些成像条件下出现的意外图像对比度问题。