College of Food Science and Technology, Huazhong Agricultural University, Wuhan, Hubei 430070, PR China; Key Laboratory of Environment Correlative Dietology, Ministry of Education, PR China.
College of Food Science and Technology, Huazhong Agricultural University, Wuhan, Hubei 430070, PR China; Key Laboratory of Environment Correlative Dietology, Ministry of Education, PR China.
Int J Biol Macromol. 2016 Oct;91:794-803. doi: 10.1016/j.ijbiomac.2016.06.011. Epub 2016 Jun 6.
Pectin was extracted from 'Tainong No. 1' mango peels, using a chelating agent-citric acid as extraction medium by ultrasound-assisted extraction (UAE) and conventional extraction (CE) at temperatures of 20 and 80°C. Chemical structures, rheological and emulsifying properties of mango peel pectins (MPPs) were comparatively studied with laboratory grade citrus pectin (CP). All MPPs exhibited higher protein content (4.74%-5.94%), degree of methoxylation (85.43-88.38%), average molecular weight (Mw, 378.4-2858kDa) than the CP, but lower galacuronic acid content (GalA, 52.21-53.35%). CE or UAE at 80°C resulted in significantly higher pectin yield than those at 20°C, while the extraction time for UAE-80°C (15min) was significantly shorter compared to CE-80°C (2h) with comparable pectin yield. Moreover, MPPs extracted at 80°C were observed with higher GalA and protein content, higher Mw, resulting in higher viscosity, better emulsifying capacity and stability, as compared to those extracted at 20°C and the CP. Therefore, these results suggested that MPPs from 'Tainong No. 1' may become a highly promising pectin with good thickening and emulsifying properties, using ultrasound-assisted citric acid as an efficient and eco-friendly extraction method.
从 '台农一号' 芒果皮中提取果胶,使用螯合剂柠檬酸作为提取介质,通过超声辅助提取(UAE)和常规提取(CE)在 20 和 80°C 的温度下进行。比较研究了芒果皮果胶(MPP)与实验室级柑橘果胶(CP)的化学结构、流变学和乳化性能。所有 MPP 的蛋白质含量(4.74%-5.94%)、甲氧基化程度(85.43-88.38%)、平均分子量(Mw,378.4-2858kDa)均高于 CP,但半乳糖醛酸含量(GalA,52.21-53.35%)较低。80°C 下的 CE 或 UAE 比 20°C 下的果胶产率显著更高,而 UAE-80°C(15min)的提取时间明显短于 CE-80°C(2h),果胶产率相当。此外,与在 20°C 下提取的果胶和 CP 相比,在 80°C 下提取的 MPP 具有更高的 GalA 和蛋白质含量、更高的 Mw,从而具有更高的粘度、更好的乳化能力和稳定性。因此,这些结果表明,使用超声辅助柠檬酸作为高效、环保的提取方法,'台农一号' 的 MPP 可能成为一种具有良好增稠和乳化性能的极具前景的果胶。