Tremsin Anton S, Ganguly Supriyo, Meco Sonia M, Pardal Goncalo R, Shinohara Takenao, Feller W Bruce
Space Sciences Laboratory, University of California at Berkeley , 7 Gauss Way, Berkeley, CA 94720, USA.
Cranfield University , Cranfield, Bedfordshire MK43 0AL, England.
J Appl Crystallogr. 2016 Jun 9;49(Pt 4):1130-1140. doi: 10.1107/S1600576716006725. eCollection 2016 Aug 1.
A nondestructive study of the internal structure and compositional gradient of dissimilar metal-alloy welds through energy-resolved neutron imaging is described in this paper. The ability of neutrons to penetrate thick metal objects (up to several cm) provides a unique possibility to examine samples which are opaque to other conventional techniques. The presence of Bragg edges in the measured neutron transmission spectra can be used to characterize the internal residual strain within the samples and some microstructural features, texture within the grains, while neutron resonance absorption provides the possibility to map the degree of uniformity in mixing of the participating alloys and intermetallic formation within the welds. In addition, voids and other defects can be revealed by the variation of neutron attenuation across the samples. This paper demonstrates the potential of neutron energy-resolved imaging to measure all these characteristics simultaneously in a single experiment with sub-mm spatial resolution. Two dissimilar alloy welds are used in this study: Al autogenously laser welded to steel, and Ti gas metal arc welded (GMAW) to stainless steel using Cu as a filler alloy. The cold metal transfer variant of the GMAW process was used in joining the Ti to the stainless steel in order to minimize the heat input. The distributions of the lattice parameter and texture variation in these welds as well as the presence of voids and defects in the melt region are mapped across the welds. The depth of the thermal front in the Al-steel weld is clearly resolved and could be used to optimize the welding process. A highly textured structure is revealed in the Ti to stainless steel joint where copper was used as a filler wire. The limited diffusion of Ti into the weld region is also verified by the resonance absorption.
本文描述了通过能量分辨中子成像对异种金属合金焊缝的内部结构和成分梯度进行无损研究。中子穿透厚金属物体(可达几厘米)的能力为检查对其他传统技术不透明的样品提供了独特的可能性。测量的中子透射谱中布拉格边缘的存在可用于表征样品内部的残余应变和一些微观结构特征、晶粒内的织构,而中子共振吸收则为绘制参与合金混合的均匀程度以及焊缝中金属间化合物形成情况提供了可能性。此外,通过样品中中子衰减的变化可以揭示孔隙和其他缺陷。本文展示了中子能量分辨成像在单次实验中以亚毫米空间分辨率同时测量所有这些特征的潜力。本研究使用了两种异种合金焊缝:铝与钢的自激光焊接,以及钛与不锈钢的气体保护金属电弧焊(GMAW),使用铜作为填充合金。在将钛与不锈钢连接时采用了GMAW工艺的冷金属过渡变体,以尽量减少热输入。绘制了这些焊缝中晶格参数和织构变化的分布以及熔合区中孔隙和缺陷的存在情况。清晰分辨出了铝 - 钢焊缝中热前沿的深度,可用于优化焊接工艺。在使用铜作为填充焊丝的钛与不锈钢接头中揭示了高度织构化的结构。通过共振吸收也证实了钛向焊缝区域的有限扩散。