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Improved synthesis of the 2-, 3-, and 4-deoxy derivatives from methyl beta-D-galactopyranoside.

作者信息

Lin T H, Kovác P, Glaudemans P J

机构信息

NIDDK, National Institutes of Health, Bethesda, Maryland 20892.

出版信息

Carbohydr Res. 1989 Jun 1;188:228-38. doi: 10.1016/0008-6215(89)84076-5.

DOI:10.1016/0008-6215(89)84076-5
PMID:2776129
Abstract
摘要

相似文献

1
Improved synthesis of the 2-, 3-, and 4-deoxy derivatives from methyl beta-D-galactopyranoside.从β-D-吡喃半乳糖苷甲酯改进合成2-、3-和4-脱氧衍生物。
Carbohydr Res. 1989 Jun 1;188:228-38. doi: 10.1016/0008-6215(89)84076-5.
2
Synthetic receptor analogues: preparation and calculated conformations of the 2-deoxy, 6-O-methyl, 6-deoxy, and 6-deoxy-6-fluoro derivatives of methyl 4-O-alpha-D-galactopyranosyl-beta-D-galactopyranoside (methyl beta-D-galabioside).
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3
Synthesis and characterization of methyl 6-O-alpha- and -beta-D-galactopyranosyl-beta-D-galactopyranoside.
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4
Unexpected formation of the 3,6-anhydro and 6-O-methyl-1-fluoro derivatives of galabiose on attempted substitution of HO-6 by fluorine in methyl 4-O-alpha-D-galactopyranosyl-beta-D-galactopyranoside (methyl beta-D-galabioside).
Carbohydr Res. 1988 May 15;176(2):287-94. doi: 10.1016/0008-6215(88)80139-3.
5
Synthesis and conformational properties of methyl 6,6-di-C-methyl-beta-D-galactopyranoside. Probes for the combining sites of D-galactosyl-binding proteins.
Carbohydr Res. 1983 Aug 16;120:43-53. doi: 10.1016/0008-6215(83)88005-7.
6
2-Substituted methyl alpha-D-galactopyranosides: synthesis and binding affinity for the A and B subunits of the Griffonia simplicifolia I isolectins.
Carbohydr Res. 1985 Jul 1;140(1):37-49. doi: 10.1016/0008-6215(85)85047-3.
7
Preparation and calculated conformations of the 2'-, 3'-, 4'-, and 6'-deoxy, 3'-O-methyl, 4'-epi, and 4'- and 6'-deoxy-fluoro derivatives of methyl 4-O-alpha-D-galactopyranosyl-beta-D-galactopyranoside (methyl beta-D-galabioside).4-O-α-D-吡喃半乳糖基-β-D-吡喃半乳糖苷甲酯（β-D-半乳糖二糖苷甲酯）的2'-、3'-、4'-和6'-脱氧、3'-O-甲基、4'-表位异构体以及4'-和6'-脱氧氟代衍生物的制备与计算构象
Carbohydr Res. 1989 Feb 1;185(2):171-90. doi: 10.1016/0008-6215(89)80033-3.
8
Conversion of galactosyl residues to 6-amino derivatives for attachment of functional groups.将半乳糖基残基转化为6-氨基衍生物以连接官能团。
Methods Enzymol. 1989;179:257-61. doi: 10.1016/0076-6879(89)79126-6.
9
Preparation of two methyl deoxyfluoro-beta-D-galactopyranosides, and their interaction with galactan-specific immunoglobulin A J539 (Fab').
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10
Synthetic receptor analogues: the conformation of methyl 4-O-alpha-D-galactopyranosyl-beta-D-galactopyranoside (methyl beta-D-galabioside) and related derivatives, determined by n.m.r. and computational methods.合成受体类似物：通过核磁共振和计算方法确定的4-O-α-D-吡喃半乳糖基-β-D-吡喃半乳糖苷甲酯（β-D-半乳糖二糖苷甲酯）及相关衍生物的构象
Carbohydr Res. 1988 May 15;176(2):253-70. doi: 10.1016/0008-6215(88)80137-x.

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