Huang Jian, Ming Yin'an, Du Ying, Wang Yingru, Wang Ci'en
School of Chemistry Environmental Engineering, Wuhan Institute of Technology, Wuhan 430073, China.
J Anal Methods Chem. 2016;2016:8198235. doi: 10.1155/2016/8198235. Epub 2016 Nov 16.
This study presents the electrochemical degradation of methylene blue (MB) wastewater in a synthetic solution using three-dimensional particle electrodes. The novel particle electrodes were fabricated in this work using the lithium modified rectorite (Li-REC). The adsorption property of the fabricated particle electrodes was studied in a series of experiments. The optimum electrochemical operating conditions of plate distance, cell voltage, and concentration of electrolyte were 2 cm, 9 V, and 0.06 mol L, respectively. It was also found that microwave irradiation can effectively improve the adsorption property and electrical property of the fabricated electrodes. In addition, the scanning electron microscope (SEM) of the fabricated electrodes was investigated. The experimental results revealed the order of adsorption property and electrical property of the fabricated electrodes. So, fabricated electrodes are not only of low cost and mass produced, but also efficient to achieve decolorization of MB solution.
本研究展示了在合成溶液中使用三维粒子电极对亚甲基蓝(MB)废水进行电化学降解。在这项工作中,使用锂改性累托石(Li-REC)制备了新型粒子电极。通过一系列实验研究了所制备粒子电极的吸附性能。极板间距、电池电压和电解质浓度的最佳电化学操作条件分别为2厘米、9伏和0.06摩尔/升。还发现微波辐射可以有效改善所制备电极的吸附性能和电学性能。此外,对所制备电极进行了扫描电子显微镜(SEM)研究。实验结果揭示了所制备电极的吸附性能和电学性能顺序。因此,所制备的电极不仅成本低且可大量生产,而且能高效实现MB溶液的脱色。