Institute of Physics, Jagiellonian University, Łojasiewicza 11, 30-348 Kraków, Poland.
Institute of Microstructure Technology, Karlsruhe Institute of Technology, 76344 Eggenstein-Leopoldshafen, Germany.
Sci Rep. 2017 Mar 21;7:44944. doi: 10.1038/srep44944.
Polycapillary devices focus X-rays by means of multiple reflections of X-rays in arrays of bent glass capillaries. The size of the focal spot (typically 10-100 μm) limits the resolution of scanning, absorption and phase-contrast X-ray imaging using these devices. At the expense of a moderate resolution, polycapillary elements provide high intensity and are frequently used for X-ray micro-imaging with both synchrotrons and X-ray tubes. Recent studies have shown that the internal microstructure of such an optics can be used as a coded aperture that encodes high-resolution information about objects located inside the focal spot. However, further improvements to this variant of X-ray microscopy will require the challenging fabrication of tailored devices with a well-defined capillary microstructure. Here, we show that submicron coded aperture microscopy can be realized using a periodic grid that is placed at the output surface of a polycapillary optics. Grid-enhanced X-ray coded aperture microscopy with polycapillary optics does not rely on the specific microstructure of the optics but rather takes advantage only of its focusing properties. Hence, submicron X-ray imaging can be realized with standard polycapillary devices and existing set-ups for micro X-ray fluorescence spectroscopy.
多晶纤维器件通过在弯曲玻璃毛细管阵列中多次反射 X 射线来聚焦 X 射线。焦斑的大小(通常为 10-100μm)限制了使用这些器件进行扫描、吸收和相衬 X 射线成像的分辨率。多晶纤维元件以中等分辨率为代价提供高强度,并且经常用于同步加速器和 X 射线管的 X 射线微成像。最近的研究表明,这种光学器件的内部微观结构可用作编码孔径,对位于焦斑内的物体进行高分辨率编码。然而,要进一步改进这种 X 射线显微镜的变体,需要具有明确定义的毛细管微观结构的定制设备的挑战性制造。在这里,我们表明,可以使用放置在多晶纤维光学器件输出表面的周期性网格来实现亚微米编码孔径显微镜。具有多晶纤维光学器件的网格增强 X 射线编码孔径显微镜不依赖于光学器件的特定微观结构,而是仅利用其聚焦特性。因此,使用标准的多晶纤维器件和现有的微 X 射线荧光光谱学设置可以实现亚微米 X 射线成像。