Zucuni C P, Guilardi L F, Fraga S, May L G, Pereira G K R, Valandro L F
MSciD-PhD Graduate Programs in Oral Science, Prosthodontics Units, Federal University of Santa Maria, Santa Maria, Rio Grande do Sul State, Brazil.
MSciD-PhD Graduate Programs in Oral Science, Prosthodontics Units, Federal University of Santa Maria, Santa Maria, Rio Grande do Sul State, Brazil; MSciD Graduate Program, School of Dentistry, Meridional Faculty - IMED, Passo Fundo, Rio Grande do Sul, Brazil.
J Mech Behav Biomed Mater. 2017 Jul;71:201-208. doi: 10.1016/j.jmbbm.2017.03.013. Epub 2017 Mar 18.
This study evaluated the effects of different pre-sintering fabrication processing techniques of Y-TZP ceramic (CAD/CAM Vs. in-lab), considering surface characteristics and mechanical performance outcomes. Pre-sintered discs of Y-TZP ceramic (IPS e.max ZirCAD, Ivoclar Vivadent) were produced using different pre-sintering fabrication processing techniques: Machined- milling with a CAD/CAM system; Polished- fabrication using a cutting device followed by polishing (600 and 1200 SiC papers); Xfine- fabrication using a cutting machine followed by grinding with extra-fine diamond bur (grit size 30 μm); Fine- fabrication using a cutting machine followed by grinding with fine diamond bur (grit size 46 μm); SiC- fabrication using a cutting machine followed by grinding with 220 SiC paper. Afterwards, the discs were sintered and submitted to roughness (n=35), surface topography (n=2), phase transformation (n=2), biaxial flexural strength (n=20), and biaxial flexural fatigue strength (fatigue limit) (n=15) analyses. No monoclinic-phase content was observed in all processing techniques. It can be observed that obtaining a surface with similar characteristics to CAD/CAM milling is essential for the observation of similar mechanical performance. On this sense, grinding with fine diamond bur before sintering (Fine group) was the best mimic protocol in comparison to the CAD/CAM milling.
本研究评估了Y-TZP陶瓷不同预烧结制造工艺技术(计算机辅助设计/计算机辅助制造与实验室制作)对表面特性和机械性能结果的影响。使用不同的预烧结制造工艺技术制作了Y-TZP陶瓷(义获嘉e.max ZirCAD,义获嘉伟瓦登特公司)的预烧结圆盘:使用计算机辅助设计/计算机辅助制造系统进行加工铣削;使用切割装置制作后进行抛光(600和1200粒度的碳化硅砂纸);使用切割机制作后用超细金刚石车针(粒度30μm)进行磨削;使用切割机制作后用细金刚石车针(粒度46μm)进行磨削;使用切割机制作后用220粒度的碳化硅砂纸进行磨削。之后,对圆盘进行烧结,并进行粗糙度分析(n = 35)、表面形貌分析(n = 2)、相变分析(n = 2)、双轴弯曲强度分析(n = 20)和双轴弯曲疲劳强度(疲劳极限)分析(n = 15)。在所有加工工艺中均未观察到单斜相含量。可以看出,获得与计算机辅助设计/计算机辅助制造铣削具有相似特性的表面对于观察相似的机械性能至关重要。从这个意义上讲,与计算机辅助设计/计算机辅助制造铣削相比,烧结前用细金刚石车针进行磨削(精细组)是最佳的模拟方案。