van den Breemer Carline R G, Özcan Mutlu, Cune Marco S, van der Giezen Rianne, Kerdijk Wouter, Gresnigt Marco M M
University Medical Center Groningen, The University of Groningen, Center for Dentistry and Oral Hygiene, Department of Fixed and Removable Prosthodontics, Groningen, The Netherlands.
University Medical Center Groningen, The University of Groningen, Center for Dentistry and Oral Hygiene, Department of Fixed and Removable Prosthodontics, Groningen, The Netherlands; University of Zurich, Dental Materials Unit, Center for Dental and Oral Medicine, Clinic for Fixed and Removable Prosthodontics and Dental Materials Science, Zurich, Switzerland.
J Mech Behav Biomed Mater. 2017 Aug;72:102-109. doi: 10.1016/j.jmbbm.2017.04.002. Epub 2017 Apr 8.
Limited information is available on the effect of Immediate Dentin Sealing (IDS) on the fracture strength of indirect partial posterior restorations. This study evaluated the effect of IDS on the fracture strength and failure types of two indirect restorative materials.
Standard MOD inlay preparations were made on sound molars (N=40, n=10 per group) and randomly divided into four groups to receive the inlay materials with and without the application of IDS: Group L-IDS-: LiSiO (Lithium disilicate, IPS e.max) without IDS; Group L-IDS+: LiSiO with IDS; Group MR-IDS-: Multiphase resin composite (MR, Lava Ultimate) without IDS; MR-IDS+: MR with IDS. Inlays made of L were etched with 5% hydrofluoric acid, and MR inlays were silica coated. After silanization, they were cemented using adhesive resin cement (Variolink Esthetic DC). The specimens were thermo-mechanically aged (1.2×10 cycles, 1.7Hz, 8000 cycles, 5-55°C) and then subjected to load to failure (1 mm/min). Failure types and locations of debondings were classified. Data were statistically analyzed using ANOVA, Mann Whitney U-test and Chi-square tests (α=0.05). Two-parameter Weibull distribution values including the Weibull modulus, scale (m) and shape (0), values were calculated.
After aging conditions, no apparent changes were observed in marginal integrity but occlusal wear facets were more common with MR than with L (p<0.001). Material type and the application of IDS significantly affected the results (p=0.013). While group L-IDS- showed the lowest mean fracture strength (1358±506N) among all groups (p<0.05), application of IDS significantly increased the results significantly (L-IDS+: 2035±403N) (p=0.006). MR groups with and without IDS, did not show significant difference (MR-IDS-: 1861±423, MR-IDS+: 1702±596 N) (p=0.498). When materials without IDS are compared, L showed significantly lower results than that of MR (p=0.035). With the application of IDS, no significant difference was noted between L and MR materials (p=0.160). Weibull distribution presented the highest shape (0) for L-IDS+ (5.66) compared to those of other groups (3.01-4.76). Neither the material type (p=0.830), nor the application of IDS (p=0.54) affected the severity of the failure types. In 95% of the cases, the IDS layer left adhered on the tooth surface after fracture tests. In groups where no IDS was used, resin cement remained on the tooth surface in 44% of the cases (p=0.001). No significant differences were observed between the materials with respect to cement remnants or IDS after fracture (p=0.880). The incidence of repairable failure types (83%) was more common with L than with MR (75%) material (p>0.05).
Immediate dentin sealing improves adhesion, and thereby the fracture strength of inlays made of lithium disilicate but not that multiphase resin composite.
关于即刻牙本质封闭(IDS)对间接部分后牙修复体断裂强度的影响,目前可用信息有限。本研究评估了IDS对两种间接修复材料的断裂强度和失败类型的影响。
在完好的磨牙上制备标准的MOD嵌体(N = 40,每组n = 10),并随机分为四组,分别接受有无IDS应用的嵌体材料:L - IDS -组:无IDS的硅酸锂(二硅酸锂,IPS e.max);L - IDS +组:有IDS的硅酸锂;MR - IDS -组:无IDS的多相树脂复合材料(MR,Lava Ultimate);MR - IDS +组:有IDS的MR。L制成的嵌体用5%氢氟酸蚀刻,MR嵌体进行硅涂层处理。硅烷化后,使用粘结树脂水门汀(Variolink Esthetic DC)粘结。对标本进行热机械老化(1.2×10次循环,1.7Hz,8000次循环,5 - 55°C),然后进行加载直至破坏(1mm/min)。对脱粘的失败类型和位置进行分类。数据采用方差分析、曼 - 惠特尼U检验和卡方检验进行统计学分析(α = 0.05)。计算包括威布尔模量、尺度(m)和形状(0)值在内的双参数威布尔分布值。
在老化条件后,边缘完整性未观察到明显变化,但MR的咬合磨损面比L更常见(p < 0.001)。材料类型和IDS的应用对结果有显著影响(p = 0.013)。虽然L - IDS -组在所有组中显示出最低的平均断裂强度(1358±506N)(p < 0.05),但IDS的应用显著提高了结果(L - IDS +组:2035±403N)(p = 0.006)。有和无IDS的MR组之间没有显著差异(MR - IDS -组:1861±423,MR - IDS +组:1702±596N)(p = 0.498)。当比较无IDS的材料时,L显示出明显低于MR的结果(p = 0.035)。应用IDS后,L和MR材料之间没有显著差异(p = 0.160)。与其他组(3.01 - 4.76)相比,L - IDS +组的威布尔分布呈现出最高的形状(0)值(5.66)。材料类型(p = 0.830)和IDS的应用(p = 0.54)均未影响失败类型的严重程度。在95%的情况下,断裂试验后IDS层仍附着在牙齿表面。在未使用IDS的组中,44%的情况下树脂水门汀留在牙齿表面(p = 0.001)。断裂后,材料在水门汀残余物或IDS方面没有观察到显著差异(p = 0.880)。可修复失败类型的发生率(83%)在L材料中比MR材料(75%)更常见(p > 0.05)。
即刻牙本质封闭可改善粘结,从而提高二硅酸锂制成的嵌体的断裂强度,但对多相树脂复合材料无效。